(OC-6-23)-[2-[6-[(amino-κN)methyl]-2-pyridinyl-κN]-5-methylphenyl-κC][1,1'-(1,4-butanediyl)bis[1,1-diphenylphosphine-κP]]chlororuthenium(II)

Base Information

Chemical Name:(OC-6-23)-[2-[6-[(amino-κN)methyl]-2-pyridinyl-κN]-5-methylphenyl-κC][1,1'-(1,4-butanediyl)bis[1,1-diphenylphosphine-κP]]chlororuthenium(II)
CAS No.:870641-27-3
Molecular Formula:C₄₁H₄₁ClN₂P₂Ru
Molecular Weight:760.26
Hs Code.:

Synonyms:(OC-6-23)-[2-[6-[(amino-κN)methyl]-2-pyridinyl-κN]-5-methylphenyl-κC][1,1'-(1,4-butanediyl)bis[1,1-diphenylphosphine-κP]]chlororuthenium(II)

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Chemical Property of (OC-6-23)-[2-[6-[(amino-κN)methyl]-2-pyridinyl-κN]-5-methylphenyl-κC][1,1'-(1,4-butanediyl)bis[1,1-diphenylphosphine-κP]]chlororuthenium(II)

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Technology Process of (OC-6-23)-[2-[6-[(amino-κN)methyl]-2-pyridinyl-κN]-5-methylphenyl-κC][1,1'-(1,4-butanediyl)bis[1,1-diphenylphosphine-κP]]chlororuthenium(II)

There total 9 articles about (OC-6-23)-[2-[6-[(amino-κN)methyl]-2-pyridinyl-κN]-5-methylphenyl-κC][1,1'-(1,4-butanediyl)bis[1,1-diphenylphosphine-κP]]chlororuthenium(II) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 88496-72-4
RuCl2(1,4-bis(diphenylphosphino)butane)(PPh3)

: 870641-29-5
rac-1-[6-(4'-methylphenyl)pyridin-2-yl]methanamine

: 870641-27-3
(OC-6-23)-[2-[6-[(amino-κN)methyl]-2-pyridinyl-κN]-5-methylphenyl-κC][1,1'-(1,4-butanediyl)bis[1,1-diphenylphosphine-κP]]chlororuthenium(II)

Guidance literature:: With triethylamine; In isopropyl alcohol; at 83 ℃; for 3h;
DOI:10.1002/ejic.202000068

Reference yield: 80.0%

: 1438275-65-0
[RuCl(η⁶-p-cymene)(6-(4′-methylphenyl)-2-pyridylmethylamine)]Cl

: 7688-25-7
1,4-di(diphenylphosphino)-butane

: 870641-27-3
(OC-6-23)-[2-[6-[(amino-κN)methyl]-2-pyridinyl-κN]-5-methylphenyl-κC][1,1'-(1,4-butanediyl)bis[1,1-diphenylphosphine-κP]]chlororuthenium(II)

Guidance literature:: With triethylamine; In ethanol; for 2h; Inert atmosphere; Schlenk technique; Reflux;
DOI:10.1021/om400280m

Reference yield: 75.0%

: 15529-49-4,41756-81-4
tris(triphenylphosphine)ruthenium(II) chloride

: 870641-29-5
rac-1-[6-(4'-methylphenyl)pyridin-2-yl]methanamine

: 7688-25-7
1,4-di(diphenylphosphino)-butane

: 870641-27-3
(OC-6-23)-[2-[6-[(amino-κN)methyl]-2-pyridinyl-κN]-5-methylphenyl-κC][1,1'-(1,4-butanediyl)bis[1,1-diphenylphosphine-κP]]chlororuthenium(II)

Guidance literature:: tris(triphenylphosphine)ruthenium(II) chloride; 1,4-di(diphenylphosphino)-butane; In isopropyl alcohol; Inert atmosphere; Reflux;

rac-1-[6-(4'-methylphenyl)pyridin-2-yl]methanamine; With triethylamine; In isopropyl alcohol; for 4h; Inert atmosphere; Reflux;
DOI:10.1002/anie.202010484