C₃₀H₂₀Cl₂N₂O₂

Base Information

• Chemical Name: C₃₀H₂₀Cl₂N₂O₂
• CAS No.: 1361403-93-1
• Molecular Formula: C₃₀H₂₀Cl₂N₂O₂
• Molecular Weight: 511.407
• Mol file: 1361403-93-1.mol

Synonyms:C₃₀H₂₀Cl₂N₂O₂

Chemical Property of C₃₀H₂₀Cl₂N₂O₂

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of C₃₀H₂₀Cl₂N₂O₂

There total 1 articles about C₃₀H₂₀Cl₂N₂O₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

5-chloroindole 2,3-dione (17630-76-1) + benzyl bromide (100-39-0) → C30H20Cl2N2O2 (1361403-93-1)

Guidance literature:

5-chloroindole 2,3-dione; With piperidine; ethyl 2-cyanoacetate; In ethanol; for 2h; Reflux; Inert atmosphere;

benzyl bromide; With potassium carbonate; In N,N-dimethyl-formamide; at 20 ℃; Inert atmosphere;

DOI:10.1016/j.tet.2012.01.036

Reference yield: 97.0%

C30H20Cl2N2O2 (1361403-93-1) + buta-2,3-dienoic acid benzyl ester (187661-86-5) → benzyl (2'S,3S)-1,1''-dibenzyl-5,5''-dichloro-2,2''-dioxodispiro[indoline-3,1'-cyclopentane-2',3''-indolin]-3'-ene-3'-carboxylate

Guidance literature:

With C₄₁H₄₀F₆NO₂PSi; In toluene; at -20 ℃; enantioselective reaction; Schlenk technique; Inert atmosphere;

DOI:10.1002/anie.201900758

Reference yield: 91.0%

C30H20Cl2N2O2 (1361403-93-1) + methyl ethynyl ketone (1423-60-5) → C34H24Cl2N2O3 (1361403-94-2)

Guidance literature:

With triphenylphosphine; In tetrahydrofuran; at 20 ℃; for 5h; Inert atmosphere;

DOI:10.1016/j.tet.2012.01.036

upstream raw materials:

5-chloroindole 2,3-dione

benzyl bromide

Downstream raw materials:

C₃₄H₂₄Cl₂N₂O₃