rac-2-(cyclohex-3-en-1-yl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

Base Information

Chemical Name:rac-2-(cyclohex-3-en-1-yl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane
CAS No.:1446696-33-8
Molecular Formula:C₁₂H₂₁BO₂
Molecular Weight:208.109
Hs Code.:

Synonyms:rac-2-(cyclohex-3-en-1-yl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

Suppliers and Price of rac-2-(cyclohex-3-en-1-yl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of rac-2-(cyclohex-3-en-1-yl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of rac-2-(cyclohex-3-en-1-yl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

There total 4 articles about rac-2-(cyclohex-3-en-1-yl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: (Z)-N-((cyclohex-3-ene-1-carbonyl)oxy)-4-methoxybenzimidoyl chloride

: 73183-34-3
bis(pinacol)diborane

: 1446696-33-8
rac-2-(cyclohex-3-en-1-yl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

Guidance literature:: (Z)-N-((cyclohex-3-ene-1-carbonyl)oxy)-4-methoxybenzimidoyl chloride; bis(pinacol)diborane; With N,N,N,N,N,N-hexamethylphosphoric triamide; Ir[dF(p-t-Bu)]ppy₃; In ethyl acetate; at 25 ℃; for 14h; Inert atmosphere; Irradiation;

With 2,3-dimethyl-2,3-butane diol; triethylamine; In ethyl acetate; for 1h; Inert atmosphere;
DOI:10.1002/anie.202008138

Reference yield: 79.0%

: 1165952-91-9
cyclohexa-1,3-diene

: 25015-63-8
4,4,5,5-tetramethyl-[1,3,2]-dioxaboralane

: 1446696-33-8
rac-2-(cyclohex-3-en-1-yl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

Guidance literature:: With [1,3-bis(diphenylphosphino)propane]cobalt(II) dichloride; In diethyl ether; at 20 ℃; Reagent/catalyst; regioselective reaction; Inert atmosphere; Schlenk technique;
DOI:10.1021/jacs.8b13812

Reference yield: 77.0%

: 1165952-91-9
cyclohexa-1,3-diene

: 73183-34-3
bis(pinacol)diborane

: 1446696-33-8
rac-2-(cyclohex-3-en-1-yl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

Guidance literature:: bis(pinacol)diborane; With C₃₉H₂₄Cl₈OP₂; copper(l) chloride; sodium t-butanolate; In tetrahydrofuran; at 20 ℃; for 0.0833333h; Inert atmosphere;

cyclohexa-1,3-diene; With methanol; In tetrahydrofuran; at 60 ℃; for 5h; Inert atmosphere;
DOI:10.1002/chem.201300443