N,N′-bis(4-bromo-2,6-diisopropylphenyl)perylene-3,4:9,10-tetracarboxylic bisimide

Base Information

Chemical Name:N,N′-bis(4-bromo-2,6-diisopropylphenyl)perylene-3,4:9,10-tetracarboxylic bisimide
CAS No.:1308878-46-7
Molecular Formula:C₄₈H₄₀Br₂N₂O₄
Molecular Weight:868.665
Hs Code.:

Synonyms:N,N′-bis(4-bromo-2,6-diisopropylphenyl)perylene-3,4:9,10-tetracarboxylic bisimide

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Chemical Property of N,N′-bis(4-bromo-2,6-diisopropylphenyl)perylene-3,4:9,10-tetracarboxylic bisimide

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Technology Process of N,N′-bis(4-bromo-2,6-diisopropylphenyl)perylene-3,4:9,10-tetracarboxylic bisimide

There total 5 articles about N,N′-bis(4-bromo-2,6-diisopropylphenyl)perylene-3,4:9,10-tetracarboxylic bisimide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 80058-84-0
4-bromo-2,6-diisopropylaniline

: perylene-3,4:9,10-tetra(n-butoxy)tetracarboxylic acid tetraester

: 1308878-46-7
N,N′-bis(4-bromo-2,6-diisopropylphenyl)perylene-3,4:9,10-tetracarboxylic bisimide

Guidance literature:: With 1H-imidazole; zinc(II) chloride; at 180 ℃; for 16h;
DOI:10.1021/acs.chemmater.5b04602

Reference yield: 60.0%

: 1453905-15-1
N,N’-bis(4-bromo-2,6-diisopropyl)-4,4’-binaphthyl-1,1’,8,8’-teracarboxylic bisimide

: 1308878-46-7
N,N′-bis(4-bromo-2,6-diisopropylphenyl)perylene-3,4:9,10-tetracarboxylic bisimide

Guidance literature:: With potassium carbonate; In ethanolamine; at 100 ℃; for 19h; Inert atmosphere;
DOI:10.1021/ol401946g

Reference yield:

: 1002762-48-2
tetramethyl 4,4'-binaphthyl-1,1',8,8'-tetracarboxylate

: 1308878-46-7
N,N′-bis(4-bromo-2,6-diisopropylphenyl)perylene-3,4:9,10-tetracarboxylic bisimide

Guidance literature:: Multi-step reaction with 2 steps

1: zinc(II) chloride hexahydrate; 1H-imidazole / 24 h / 140 °C / Inert atmosphere

2: potassium carbonate / ethanolamine / 19 h / 100 °C / Inert atmosphere

With 1H-imidazole; zinc(II) chloride hexahydrate; potassium carbonate; In ethanolamine;
DOI:10.1021/ol401946g