N-(3-(4-(1-(2,3-anhydridehydroxylethyl)-5-nitrophenoxy)acetamide)propyl) methacrylamide

Base Information

Chemical Name:N-(3-(4-(1-(2,3-anhydridehydroxylethyl)-5-nitrophenoxy)acetamide)propyl) methacrylamide
CAS No.:890404-58-7
Molecular Formula:C₂₇H₂₇N₃O₁₁
Molecular Weight:569.525
Hs Code.:

Synonyms:N-(3-(4-(1-(2,3-anhydridehydroxylethyl)-5-nitrophenoxy)acetamide)propyl) methacrylamide

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Chemical Property of N-(3-(4-(1-(2,3-anhydridehydroxylethyl)-5-nitrophenoxy)acetamide)propyl) methacrylamide

Chemical Property:

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Technology Process of N-(3-(4-(1-(2,3-anhydridehydroxylethyl)-5-nitrophenoxy)acetamide)propyl) methacrylamide

There total 6 articles about N-(3-(4-(1-(2,3-anhydridehydroxylethyl)-5-nitrophenoxy)acetamide)propyl) methacrylamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 890404-56-5
N-(3-(4-acetyl-2-methoxy-5-nitrophenoxy)acetamide)propyl methacrylamide

: 1204-28-0
trimellitic anhydride acid chloride

: 890404-58-7
N-(3-(4-(1-(2,3-anhydridehydroxylethyl)-5-nitrophenoxy)acetamide)propyl) methacrylamide

Guidance literature:: With pyridine; In dichloromethane; at 0 - 20 ℃;

Reference yield:

: 188891-12-5
(4-acetyl-2-methoxy-phenoxy)acetic acid tert-butyl ester

: 890404-58-7
N-(3-(4-(1-(2,3-anhydridehydroxylethyl)-5-nitrophenoxy)acetamide)propyl) methacrylamide

Guidance literature:: Multi-step reaction with 5 steps

1: nitric acid; acetic anhydride / 6 h / 0 - 20 °C

2: dicyclohexyl-carbodiimide / dichloromethane / 1 h / 20 °C / Inert atmosphere

3: triethylamine / dichloromethane / 48 h / 20 °C / Inert atmosphere

4: sodium tetrahydroborate / ethanol / 0 - 20 °C

5: pyridine / dichloromethane / 0 - 20 °C / Inert atmosphere

With pyridine; sodium tetrahydroborate; nitric acid; acetic anhydride; triethylamine; dicyclohexyl-carbodiimide; In ethanol; dichloromethane;
DOI:10.1039/b922613c

Reference yield:

: C₁₅H₁₄N₂O₉

: 890404-58-7
N-(3-(4-(1-(2,3-anhydridehydroxylethyl)-5-nitrophenoxy)acetamide)propyl) methacrylamide

Guidance literature:: Multi-step reaction with 3 steps

1: triethylamine / dichloromethane / 48 h / 20 °C / Inert atmosphere

2: sodium tetrahydroborate / ethanol / 0 - 20 °C

3: pyridine / dichloromethane / 0 - 20 °C / Inert atmosphere

With pyridine; sodium tetrahydroborate; triethylamine; In ethanol; dichloromethane;
DOI:10.1039/b922613c