N-(3-(4-acetyl-2-methoxy-5-nitrophenoxy)acetamide)propyl methacrylamide

Base Information

Chemical Name:N-(3-(4-acetyl-2-methoxy-5-nitrophenoxy)acetamide)propyl methacrylamide
CAS No.:890404-56-5
Molecular Formula:C₁₈H₂₃N₃O₇
Molecular Weight:393.397
Hs Code.:

Synonyms:N-(3-(4-acetyl-2-methoxy-5-nitrophenoxy)acetamide)propyl methacrylamide

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Chemical Property of N-(3-(4-acetyl-2-methoxy-5-nitrophenoxy)acetamide)propyl methacrylamide

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Technology Process of N-(3-(4-acetyl-2-methoxy-5-nitrophenoxy)acetamide)propyl methacrylamide

There total 4 articles about N-(3-(4-acetyl-2-methoxy-5-nitrophenoxy)acetamide)propyl methacrylamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 188891-13-6
2-(4-acetyl-2-methoxy-5-nitrophenoxy)acetic acid

: 72607-53-5
N-(3-aminopropyl)methacrylamide hydrochloride

: 890404-56-5
N-(3-(4-acetyl-2-methoxy-5-nitrophenoxy)acetamide)propyl methacrylamide

Guidance literature:: 2-(4-acetyl-2-methoxy-5-nitrophenoxy)acetic acid; With 1-hydroxy-pyrrolidine-2,5-dione; dicyclohexyl-carbodiimide; In dichloromethane; at 20 ℃; for 1h;

N-(3-aminopropyl)methacrylamide hydrochloride; With triethylamine; In dichloromethane; at 20 ℃; for 48h;

Reference yield:

: 188891-12-5
(4-acetyl-2-methoxy-phenoxy)acetic acid tert-butyl ester

: 890404-56-5
N-(3-(4-acetyl-2-methoxy-5-nitrophenoxy)acetamide)propyl methacrylamide

Guidance literature:: Multi-step reaction with 3 steps

1: nitric acid; acetic anhydride / 6 h / 0 - 20 °C

2: dicyclohexyl-carbodiimide / dichloromethane / 1 h / 20 °C / Inert atmosphere

3: triethylamine / dichloromethane / 48 h / 20 °C / Inert atmosphere

With nitric acid; acetic anhydride; triethylamine; dicyclohexyl-carbodiimide; In dichloromethane;
DOI:10.1039/b922613c

Reference yield:

: 188891-13-6
2-(4-acetyl-2-methoxy-5-nitrophenoxy)acetic acid

: 890404-56-5
N-(3-(4-acetyl-2-methoxy-5-nitrophenoxy)acetamide)propyl methacrylamide

Guidance literature:: Multi-step reaction with 2 steps

1: dicyclohexyl-carbodiimide / dichloromethane / 1 h / 20 °C / Inert atmosphere

2: triethylamine / dichloromethane / 48 h / 20 °C / Inert atmosphere

With triethylamine; dicyclohexyl-carbodiimide; In dichloromethane;
DOI:10.1039/b922613c