C₄₄H₃₃Br₂NO₂

Base Information

Chemical Name:C₄₄H₃₃Br₂NO₂
CAS No.:1449490-07-6
Molecular Formula:C₄₄H₃₃Br₂NO₂
Molecular Weight:767.56
Hs Code.:

C<sub>44</sub>H<sub>33</sub>Br<sub>2</sub>NO<sub>2</sub>

Synonyms:C₄₄H₃₃Br₂NO₂

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Chemical Property of C₄₄H₃₃Br₂NO₂

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Technology Process of C₄₄H₃₃Br₂NO₂

There total 4 articles about C₄₄H₃₃Br₂NO₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 51.0%

: 58556-75-5
2,7-dibromonaphthalene

: 1449490-10-1
C₃₆H₄₅B₂NO₆

: 1449490-07-6
C₄₄H₃₃Br₂NO₂

Guidance literature:: With dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; potassium carbonate; In dimethyl sulfoxide; at 80 ℃;
DOI:10.1016/j.tetlet.2013.07.025

Reference yield:

: 1449490-09-8
C₂₄H₂₁Br₂NO₂

: 1449490-07-6
C₄₄H₃₃Br₂NO₂

Guidance literature:: Multi-step reaction with 2 steps

1: dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; potassium acetate / 1,4-dioxane / 3 h / 80 °C

2: dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; potassium carbonate / dimethyl sulfoxide / 80 °C

With dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; potassium acetate; potassium carbonate; In 1,4-dioxane; dimethyl sulfoxide;
DOI:10.1016/j.tetlet.2013.07.025

Reference yield:

: 81-84-5
1,8-Naphthalic anhydride

: 1449490-07-6
C₄₄H₃₃Br₂NO₂

Guidance literature:: Multi-step reaction with 4 steps

1.1: N-Bromosuccinimide; sulfuric acid / 6 h / 60 °C

2.1: acetic acid / 4 h / Reflux

2.2: 4 h / Reflux

3.1: dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; potassium acetate / 1,4-dioxane / 3 h / 80 °C

4.1: dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; potassium carbonate / dimethyl sulfoxide / 80 °C

With N-Bromosuccinimide; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; sulfuric acid; potassium acetate; potassium carbonate; acetic acid; In 1,4-dioxane; dimethyl sulfoxide;
DOI:10.1016/j.tetlet.2013.07.025