C₃₅H₄₂N₂NiO

Base Information

Chemical Name:C₃₅H₄₂N₂NiO
CAS No.:1364809-13-1
Molecular Formula:C₃₅H₄₂N₂NiO
Molecular Weight:565.421
Hs Code.:

C<sub>35</sub>H<sub>42</sub>N<sub>2</sub>NiO

Synonyms:C₃₅H₄₂N₂NiO

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Chemical Property of C₃₅H₄₂N₂NiO

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Technology Process of C₃₅H₄₂N₂NiO

There total 2 articles about C₃₅H₄₂N₂NiO which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 110-86-1
pyridine

: dimethyl(tetramethylethylenediamine)nickel(II)

: 1364809-10-8
(CH(CH₃)2)2C₆H₃NCHC(CH₃)3OHC₆H₂C₆H₅

: 1364809-13-1
C₃₅H₄₂N₂NiO

Guidance literature:: In diethyl ether; at -35 - 20 ℃;

Reference yield:

: 110-86-1
pyridine

: dimethyl(tetramethylethylenediamine)nickel(II)

: 1364809-10-8
(CH(CH₃)2)2C₆H₃NCHC(CH₃)3OHC₆H₂C₆H₅

: 1364809-13-1
(CH(CH₃)2)2C₆H₃NCHC(CH₃)3OC₆H₂C₆H₅NiCH₃(C₅H₅N)

Guidance literature:: In diethyl ether; byproducts: CH4, N,N,N',N'-tetramethylethylenediamine; under an inert atm.; a soln. of a ligand (1 equiv.) in Et2O and a soln. of Ni-contg. compd. (1.1 equivs.) in Et2O were cooled to ca. -35°C; the soln. of the ligand was added to the soln. of Ni-contg. compd.; pyridine (10 equivs.) was added; after stirring for 6 h at room temp. volatiles were removed under vac.; the suspn. was washed over Celite with hexanes; volatiles were removed from the filtrate under vac.; pptn. from pentane;
DOI:10.1021/om2011694