C₁₀H₁₁NO

Base Information

• Chemical Name: C₁₀H₁₁NO
• CAS No.: 952108-79-1
• Molecular Formula: C₁₀H₁₁NO
• Molecular Weight: 161.203
• Mol file: 952108-79-1.mol

Synonyms:C₁₀H₁₁NO

Chemical Property of C₁₀H₁₁NO

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of C₁₀H₁₁NO

There total 2 articles about C₁₀H₁₁NO which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

2-(1-methylethenyl)benzaldehyde (23417-79-0) → C10H11NO (952108-79-1)

Guidance literature:

With sodium hydroxide; hydroxylamine hydrochloride; In dichloromethane; at 20 ℃; for 5h;

DOI:10.1055/s-2007-984900

Reference yield:

1-chloro-2-(prop-1-en-2-yl)benzene (3609-45-8) → C10H11NO (952108-79-1)

Guidance literature:

Multi-step reaction with 2 steps

1.1: Mg / tetrahydrofuran

1.2: 74 percent / tetrahydrofuran / 20 °C

2.1: 85 percent / NH₂OH*HCl; aq. NaOH / CH₂Cl₂ / 5 h / 20 °C

With sodium hydroxide; hydroxylamine hydrochloride; magnesium; In tetrahydrofuran; dichloromethane;

DOI:10.1055/s-2007-984900

Reference yield:

C10H11NO (952108-79-1) → C16H17NO

Guidance literature:

Multi-step reaction with 3 steps

1: NaBH₃CN; aq. HCl / methanol / 1 h / 20 °C / pH 3

2: 318 mg / aq. NH₄OH; air / Cu(OAc)2 / methanol / 2 h

3: diethyl ether / 20 °C

With hydrogenchloride; ammonium hydroxide; air; sodium cyanoborohydride; copper diacetate; In methanol; diethyl ether;

DOI:10.1055/s-2007-984900

upstream raw materials:

2-(1-methylethenyl)benzaldehyde

1-chloro-2-(prop-1-en-2-yl)benzene

Refernces