di[(1-(2-phenylindol-1-yl)-2-chloromethyl-2-methyl)propoxy]diphenylsilane

Base Information

Chemical Name:di[(1-(2-phenylindol-1-yl)-2-chloromethyl-2-methyl)propoxy]diphenylsilane
CAS No.:1314235-54-5
Molecular Formula:C₅₀H₄₈Cl₂N₂O₂Si
Molecular Weight:807.935
Hs Code.:

Synonyms:di[(1-(2-phenylindol-1-yl)-2-chloromethyl-2-methyl)propoxy]diphenylsilane

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Chemical Property of di[(1-(2-phenylindol-1-yl)-2-chloromethyl-2-methyl)propoxy]diphenylsilane

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Technology Process of di[(1-(2-phenylindol-1-yl)-2-chloromethyl-2-methyl)propoxy]diphenylsilane

There total 2 articles about di[(1-(2-phenylindol-1-yl)-2-chloromethyl-2-methyl)propoxy]diphenylsilane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 1069473-27-3
3-(2-phenylindol-1-ylmethyl)-3-methyloxetane

: 80-10-4
diphenylsilyl dichloride

: 1314235-54-5
di[(1-(2-phenylindol-1-yl)-2-chloromethyl-2-methyl)propoxy]diphenylsilane

Guidance literature:: With tetrabutylammomium bromide; In tetrahydrofuran; at 20 - 50 ℃; for 48.5h;
DOI:10.1016/j.dyepig.2011.03.020

Reference yield:

: 78385-26-9
3-bromomethyl-3-methyloxetane

: 948-65-2
2-phenyl-indole

: 1314235-54-5
di[(1-(2-phenylindol-1-yl)-2-chloromethyl-2-methyl)propoxy]diphenylsilane

Guidance literature:: Multi-step reaction with 2 steps

1: phase transfer catalyst / Alkaline conditions

2: tetrabutylammomium bromide / tetrahydrofuran / 48.5 h / 20 - 50 °C

With tetrabutylammomium bromide; In tetrahydrofuran;
DOI:10.1016/j.dyepig.2011.03.020