Technology Process of methyl 3,5-dichloro-2,4,6-trifluorobenzoate
There total 1 articles about methyl 3,5-dichloro-2,4,6-trifluorobenzoate which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 2 steps
1: KF / 280 - 285 °C
With
potassium fluoride;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: N-ethyl-N,N-diisopropylamine; tris[2-phenylpyridinato-C2,N]iridium(III) / acetonitrile / 55 h / 65 °C / Sealed tube; Inert atmosphere; Photolysis
2: lithium aluminium tetrahydride / tetrahydrofuran / 16 h / 0 - 20 °C
3: carbon tetrabromide; triphenylphosphine / diethyl ether / 2 h / 25 °C
With
tris[2-phenylpyridinato-C2,N]iridium(III); lithium aluminium tetrahydride; carbon tetrabromide; N-ethyl-N,N-diisopropylamine; triphenylphosphine;
In
tetrahydrofuran; diethyl ether; acetonitrile;
- Guidance literature:
-
Multi-step reaction with 2 steps
1: N-ethyl-N,N-diisopropylamine; tris[2-phenylpyridinato-C2,N]iridium(III) / acetonitrile / 55 h / 65 °C / Sealed tube; Inert atmosphere; Photolysis
2: lithium aluminium tetrahydride / tetrahydrofuran / 16 h / 0 - 20 °C
With
tris[2-phenylpyridinato-C2,N]iridium(III); lithium aluminium tetrahydride; N-ethyl-N,N-diisopropylamine;
In
tetrahydrofuran; acetonitrile;
