(S)-3-Benzyloxycarbonylamino-N-{(R)-1-[(1-methyl-cyclohexanecarbonyl)-amino]-ethyl}-succinamic acid benzyl ester

Base Information

• Chemical Name: (S)-3-Benzyloxycarbonylamino-N-{(R)-1-[(1-methyl-cyclohexanecarbonyl)-amino]-ethyl}-succinamic acid benzyl ester
• CAS No.: 96188-64-6
• Molecular Formula: C₂₉H₃₇N₃O₆
• Molecular Weight: 523.629

Synonyms:(S)-3-Benzyloxycarbonylamino-N-{(R)-1-[(1-methyl-cyclohexanecarbonyl)-amino]-ethyl}-succinamic acid benzyl ester

Chemical Property of (S)-3-Benzyloxycarbonylamino-N-{(R)-1-[(1-methyl-cyclohexanecarbonyl)-amino]-ethyl}-succinamic acid benzyl ester

Chemical Property:

Purity/Quality:

98% ^*data from raw suppliers

Safty Information:

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Technology Process of (S)-3-Benzyloxycarbonylamino-N-{(R)-1-[(1-methyl-cyclohexanecarbonyl)-amino]-ethyl}-succinamic acid benzyl ester

There total 2 articles about (S)-3-Benzyloxycarbonylamino-N-{(R)-1-[(1-methyl-cyclohexanecarbonyl)-amino]-ethyl}-succinamic acid benzyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(S)-3-Benzyloxycarbonylamino-N-((R)-1-carbamoyl-ethyl)-succinamic acid benzyl ester → (S)-3-Benzyloxycarbonylamino-N-{(R)-1-[(1-methyl-cyclohexanecarbonyl)-amino]-ethyl}-succinamic acid benzyl ester (96188-64-6)

Guidance literature:

Multi-step reaction with 2 steps

1: 1.) benzene, 2.) HCl

2: KHCO₃

With hydrogenchloride; bis-(trifluoroacetoxy)-iodo-benzene; potassium hydrogencarbonate;

DOI:10.1021/ja00306a051

Reference yield:

(S)-N-((R)-1-Amino-ethyl)-3-benzyloxycarbonylamino-succinamic acid benzyl ester; hydrochloride + 1-methyl-1-cyclohexancarboxylic acid chloride (2890-61-1) → (S)-3-Benzyloxycarbonylamino-N-{(R)-1-[(1-methyl-cyclohexanecarbonyl)-amino]-ethyl}-succinamic acid benzyl ester (96188-64-6)

Guidance literature:

With potassium hydrogencarbonate;

DOI:10.1021/ja00306a051

Reference yield:

(S)-3-Benzyloxycarbonylamino-N-{(R)-1-[(1-methyl-cyclohexanecarbonyl)-amino]-ethyl}-succinamic acid benzyl ester (96188-64-6) → (S)-3-Amino-N-{(R)-1-[(1-methyl-cyclohexanecarbonyl)-amino]-ethyl}-succinamic acid

Guidance literature:

With hydrogen; palladium on activated charcoal;

DOI:10.1021/ja00306a051

upstream raw materials:

1-methyl-1-cyclohexancarboxylic acid chloride

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