3-(formyl)-1-(phenoxycarbonyl)-5-(triisopropylsilyl)-1,2,3,4-tetrahydropyridine

Base Information

Chemical Name:3-(formyl)-1-(phenoxycarbonyl)-5-(triisopropylsilyl)-1,2,3,4-tetrahydropyridine
CAS No.:372965-36-1
Molecular Formula:C₂₂H₃₃NO₃Si
Molecular Weight:387.594
Hs Code.:

Synonyms:3-(formyl)-1-(phenoxycarbonyl)-5-(triisopropylsilyl)-1,2,3,4-tetrahydropyridine

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Chemical Property of 3-(formyl)-1-(phenoxycarbonyl)-5-(triisopropylsilyl)-1,2,3,4-tetrahydropyridine

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Technology Process of 3-(formyl)-1-(phenoxycarbonyl)-5-(triisopropylsilyl)-1,2,3,4-tetrahydropyridine

There total 6 articles about 3-(formyl)-1-(phenoxycarbonyl)-5-(triisopropylsilyl)-1,2,3,4-tetrahydropyridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 3-hydroxymethyl-5-triisopropylsilanyl-3,4-dihydro-2H-pyridine-1-carboxylic acid phenyl ester

: 372965-36-1
3-(formyl)-1-(phenoxycarbonyl)-5-(triisopropylsilyl)-1,2,3,4-tetrahydropyridine

Guidance literature:: DOI:10.1021/ol016556o

Reference yield:

: 123506-73-0
3-(triisopropylsilyl)pyridine

: 372965-36-1
3-(formyl)-1-(phenoxycarbonyl)-5-(triisopropylsilyl)-1,2,3,4-tetrahydropyridine

Guidance literature:: Multi-step reaction with 5 steps

1: 71 percent / Bu₃SnH

2: 81 percent / POCl₃

3: NaBH₄; CeCl₃

4: H₂ / Pd(OH)2/C

With sodium tetrahydroborate; cerium(III) chloride; hydrogen; tri-n-butyl-tin hydride; trichlorophosphate; palladium dihydroxide; 2: Vilsmeier-Haack reaction / 3: Luche reduction / 5: Swern oxidation;
DOI:10.1021/ol016556o

Reference yield:

: 1885-14-9
phenyl chloroformate

: 372965-36-1
3-(formyl)-1-(phenoxycarbonyl)-5-(triisopropylsilyl)-1,2,3,4-tetrahydropyridine

Guidance literature:: Multi-step reaction with 5 steps

1: 71 percent / Bu₃SnH

2: 81 percent / POCl₃

3: NaBH₄; CeCl₃

4: H₂ / Pd(OH)2/C

With sodium tetrahydroborate; cerium(III) chloride; hydrogen; tri-n-butyl-tin hydride; trichlorophosphate; palladium dihydroxide; 2: Vilsmeier-Haack reaction / 3: Luche reduction / 5: Swern oxidation;
DOI:10.1021/ol016556o