2-(3'-N,O-di(tert-butoxycarbonyl)hydroxylaminopropyl)cyclohex-2-en-1-one

Base Information

Chemical Name:2-(3'-N,O-di(tert-butoxycarbonyl)hydroxylaminopropyl)cyclohex-2-en-1-one
CAS No.:608532-70-3
Molecular Formula:C₁₉H₃₁NO₆
Molecular Weight:369.458
Hs Code.:

Synonyms:2-(3'-N,O-di(tert-butoxycarbonyl)hydroxylaminopropyl)cyclohex-2-en-1-one

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Chemical Property of 2-(3'-N,O-di(tert-butoxycarbonyl)hydroxylaminopropyl)cyclohex-2-en-1-one

Chemical Property:

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Technology Process of 2-(3'-N,O-di(tert-butoxycarbonyl)hydroxylaminopropyl)cyclohex-2-en-1-one

There total 3 articles about 2-(3'-N,O-di(tert-butoxycarbonyl)hydroxylaminopropyl)cyclohex-2-en-1-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 608532-78-1
2-(3'-N,O-di(tert-butoxycarbonyl)hydroxylaminopropyl)-2-(phenylselenyl)-cyclohexanone

: 608532-70-3
2-(3'-N,O-di(tert-butoxycarbonyl)hydroxylaminopropyl)cyclohex-2-en-1-one

Guidance literature:: With dihydrogen peroxide; triethylamine; In dichloromethane; for 1h; Heating;
DOI:10.1021/jo035004b

Reference yield:

: 85006-25-3
N,N-di(tert-butoxycarbonyl)hydroxylamine

: 608532-70-3
2-(3'-N,O-di(tert-butoxycarbonyl)hydroxylaminopropyl)cyclohex-2-en-1-one

Guidance literature:: Multi-step reaction with 3 steps

1: 97 percent / K₂CO₃ / dimethylformamide / 24 h / 20 °C

2: 80 percent / AgOTf / benzene / 0.5 h

3: 91 percent / Et₃N; aq. H₂O₂ / CH₂Cl₂ / 1 h / Heating

With dihydrogen peroxide; silver trifluoromethanesulfonate; potassium carbonate; triethylamine; In dichloromethane; N,N-dimethyl-formamide; benzene;
DOI:10.1021/jo035004b

Reference yield:

: 608532-77-0
1-acetoxy-2-(3'-N,O-di(tert-butoxycarbonyl)hydroxylaminopropyl)-1-cyclohexene

: 608532-70-3
2-(3'-N,O-di(tert-butoxycarbonyl)hydroxylaminopropyl)cyclohex-2-en-1-one

Guidance literature:: Multi-step reaction with 2 steps

1: 80 percent / AgOTf / benzene / 0.5 h

2: 91 percent / Et₃N; aq. H₂O₂ / CH₂Cl₂ / 1 h / Heating

With dihydrogen peroxide; silver trifluoromethanesulfonate; triethylamine; In dichloromethane; benzene;
DOI:10.1021/jo035004b