1-acetoxy-2-(3'-N,O-di(tert-butoxycarbonyl)hydroxylaminopropyl)-1-cyclohexene

Base Information

Chemical Name:1-acetoxy-2-(3'-N,O-di(tert-butoxycarbonyl)hydroxylaminopropyl)-1-cyclohexene
CAS No.:608532-77-0
Molecular Formula:C₂₁H₃₅NO₇
Molecular Weight:413.511
Hs Code.:

Synonyms:1-acetoxy-2-(3'-N,O-di(tert-butoxycarbonyl)hydroxylaminopropyl)-1-cyclohexene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-acetoxy-2-(3'-N,O-di(tert-butoxycarbonyl)hydroxylaminopropyl)-1-cyclohexene

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Technology Process of 1-acetoxy-2-(3'-N,O-di(tert-butoxycarbonyl)hydroxylaminopropyl)-1-cyclohexene

There total 1 articles about 1-acetoxy-2-(3'-N,O-di(tert-butoxycarbonyl)hydroxylaminopropyl)-1-cyclohexene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 85006-25-3
N,N-di(tert-butoxycarbonyl)hydroxylamine

: 1-acetoxy-2-(3'-iodopropyl)-1-cyclohexene

: 608532-77-0
1-acetoxy-2-(3'-N,O-di(tert-butoxycarbonyl)hydroxylaminopropyl)-1-cyclohexene

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; at 20 ℃; for 24h;
DOI:10.1021/jo035004b

Reference yield: 80.0%

: 5707-04-0
Phenylselenyl chloride

: 608532-77-0
1-acetoxy-2-(3'-N,O-di(tert-butoxycarbonyl)hydroxylaminopropyl)-1-cyclohexene

: 608532-78-1
2-(3'-N,O-di(tert-butoxycarbonyl)hydroxylaminopropyl)-2-(phenylselenyl)-cyclohexanone

Guidance literature:: With silver trifluoromethanesulfonate; In benzene; for 0.5h;
DOI:10.1021/jo035004b

Reference yield:

: 608532-77-0
1-acetoxy-2-(3'-N,O-di(tert-butoxycarbonyl)hydroxylaminopropyl)-1-cyclohexene

: 608532-70-3
2-(3'-N,O-di(tert-butoxycarbonyl)hydroxylaminopropyl)cyclohex-2-en-1-one

Guidance literature:: Multi-step reaction with 2 steps

1: 80 percent / AgOTf / benzene / 0.5 h

2: 91 percent / Et₃N; aq. H₂O₂ / CH₂Cl₂ / 1 h / Heating

With dihydrogen peroxide; silver trifluoromethanesulfonate; triethylamine; In dichloromethane; benzene;
DOI:10.1021/jo035004b