(R)-4-(nitrooxy)butyl 2-((5-(1,2-dithiolan-3-yl)pentanoyl)oxy)benzoate

Base Information

Chemical Name:(R)-4-(nitrooxy)butyl 2-((5-(1,2-dithiolan-3-yl)pentanoyl)oxy)benzoate
CAS No.:1357392-70-1
Molecular Formula:C₁₉H₂₅NO₇S₂
Molecular Weight:443.542
Hs Code.:

Synonyms:(R)-4-(nitrooxy)butyl 2-((5-(1,2-dithiolan-3-yl)pentanoyl)oxy)benzoate

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Chemical Property of (R)-4-(nitrooxy)butyl 2-((5-(1,2-dithiolan-3-yl)pentanoyl)oxy)benzoate

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Technology Process of (R)-4-(nitrooxy)butyl 2-((5-(1,2-dithiolan-3-yl)pentanoyl)oxy)benzoate

There total 3 articles about (R)-4-(nitrooxy)butyl 2-((5-(1,2-dithiolan-3-yl)pentanoyl)oxy)benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 478163-51-8
4-(nitrooxy) butyl 2-hydroxybenzoate

: 1200-22-2
(R)-1,2-dithiolane-3-pentanoic acid

: 1357392-70-1
(R)-4-(nitrooxy)butyl 2-((5-(1,2-dithiolan-3-yl)pentanoyl)oxy)benzoate

Guidance literature:: With dmap; dicyclohexyl-carbodiimide; In dichloromethane; at 20 ℃; for 6h;
DOI:10.1021/ml300002m

Reference yield:

: 50-78-2,98201-60-6
aspirin

: 1357392-70-1
(R)-4-(nitrooxy)butyl 2-((5-(1,2-dithiolan-3-yl)pentanoyl)oxy)benzoate

Guidance literature:: Multi-step reaction with 3 steps

1: dmap; dicyclohexyl-carbodiimide / dichloromethane / 6 h / 20 °C

2: methanol; potassium carbonate / tetrahydrofuran / 0.25 h / 20 °C

3: dmap; dicyclohexyl-carbodiimide / dichloromethane / 6 h / 20 °C

With methanol; dmap; potassium carbonate; dicyclohexyl-carbodiimide; In tetrahydrofuran; dichloromethane;
DOI:10.1021/ml300002m

Reference yield:

: acetylsalicylic acid 4-(nitroxy)butyl ester

: 1357392-70-1
(R)-4-(nitrooxy)butyl 2-((5-(1,2-dithiolan-3-yl)pentanoyl)oxy)benzoate

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate / methanol; tetrahydrofuran / 0.25 h / 20 °C

2: dicyclohexyl-carbodiimide; dmap / dichloromethane / 6 h / 20 °C

With dmap; potassium carbonate; dicyclohexyl-carbodiimide; In tetrahydrofuran; methanol; dichloromethane;