{4-[4-(2-Ethyl-butyrylamino)-2-fluoro-phenyl]-piperazin-1-yl}-phenyl-acetic acid methyl ester

Base Information

Chemical Name:{4-[4-(2-Ethyl-butyrylamino)-2-fluoro-phenyl]-piperazin-1-yl}-phenyl-acetic acid methyl ester
CAS No.:935855-30-4
Molecular Formula:C₂₅H₃₂FN₃O₃
Molecular Weight:441.546
Hs Code.:

Synonyms:{4-[4-(2-Ethyl-butyrylamino)-2-fluoro-phenyl]-piperazin-1-yl}-phenyl-acetic acid methyl ester

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Chemical Property of {4-[4-(2-Ethyl-butyrylamino)-2-fluoro-phenyl]-piperazin-1-yl}-phenyl-acetic acid methyl ester

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Technology Process of {4-[4-(2-Ethyl-butyrylamino)-2-fluoro-phenyl]-piperazin-1-yl}-phenyl-acetic acid methyl ester

There total 1 articles about {4-[4-(2-Ethyl-butyrylamino)-2-fluoro-phenyl]-piperazin-1-yl}-phenyl-acetic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 57.0%

: 88-09-5
2-Ethylbutanoic acid

: 935855-32-6
[4-(4-amino-2-fluoro-phenyl)-piperazin-1-yl]-phenyl-acetic acid methyl ester

: 935855-30-4
{4-[4-(2-Ethyl-butyrylamino)-2-fluoro-phenyl]-piperazin-1-yl}-phenyl-acetic acid methyl ester

Guidance literature:: 2-Ethylbutanoic acid; With benzotriazol-1-ol; In dichloromethane; at 20 ℃; for 0.25h; not specified

[4-(4-amino-2-fluoro-phenyl)-piperazin-1-yl]-phenyl-acetic acid methyl ester; In dichloromethane; at 20 ℃; for 16h;

Reference yield:

: 935855-30-4
{4-[4-(2-Ethyl-butyrylamino)-2-fluoro-phenyl]-piperazin-1-yl}-phenyl-acetic acid methyl ester

: 127-06-0
acetone oxime

: 1163126-16-6
2-ethyl-N-(3-fluoro-4-(4-((3-methylisoxazol-5-yl)(phenyl)methyl)piperazin-1-yl)phenyl)butyramide

Guidance literature:: acetone oxime; With n-butyllithium; In tetrahydrofuran; hexane; at 0 ℃; for 2h;

{4-[4-(2-Ethyl-butyrylamino)-2-fluoro-phenyl]-piperazin-1-yl}-phenyl-acetic acid methyl ester; In tetrahydrofuran; hexane; at 0 - 20 ℃; for 17h;

With sulfuric acid; sodium hydrogencarbonate; more than 3 stages;