tert-butyl 3-[(2-chloroethyl)(2-hydroxyethyl)amino]-2,6-dinitrobenzoate

Base Information

Chemical Name:tert-butyl 3-[(2-chloroethyl)(2-hydroxyethyl)amino]-2,6-dinitrobenzoate
CAS No.:944088-76-0
Molecular Formula:C₁₅H₂₀ClN₃O₇
Molecular Weight:389.793
Hs Code.:

Synonyms:tert-butyl 3-[(2-chloroethyl)(2-hydroxyethyl)amino]-2,6-dinitrobenzoate

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Chemical Property of tert-butyl 3-[(2-chloroethyl)(2-hydroxyethyl)amino]-2,6-dinitrobenzoate

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Technology Process of tert-butyl 3-[(2-chloroethyl)(2-hydroxyethyl)amino]-2,6-dinitrobenzoate

There total 2 articles about tert-butyl 3-[(2-chloroethyl)(2-hydroxyethyl)amino]-2,6-dinitrobenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 51.0%

: 1072-52-2
2-(1-aziridine)ethanol

: 944088-65-7
tert-butyl 3-chloro-2,6-dinitrobenzoate

: 944088-76-0
tert-butyl 3-[(2-chloroethyl)(2-hydroxyethyl)amino]-2,6-dinitrobenzoate

Guidance literature:: With lithium chloride; In N,N-dimethyl-formamide; cooling;
DOI:10.1016/j.tet.2007.04.044

Reference yield:

: 150272-17-6
3-chloro-2,6-dinitrobenzoic acid

: 944088-76-0
tert-butyl 3-[(2-chloroethyl)(2-hydroxyethyl)amino]-2,6-dinitrobenzoate

Guidance literature:: Multi-step reaction with 2 steps

1: 68 percent / aq. HClO₄ / 6 h / 35 °C

2: 51 percent / LiCl / dimethylformamide / cooling

With perchloric acid; lithium chloride; In N,N-dimethyl-formamide;
DOI:10.1016/j.tet.2007.04.044

Reference yield: 88.0%

: 944088-76-0
tert-butyl 3-[(2-chloroethyl)(2-hydroxyethyl)amino]-2,6-dinitrobenzoate

: 124-63-0
methanesulfonyl chloride

: tert-butyl 3-[(2-chloroethyl)[2-[(methylsulfonyl)oxy]ethyl]amino]-2,6-dinitrobenzoate

Guidance literature:: tert-butyl 3-[(2-chloroethyl)(2-hydroxyethyl)amino]-2,6-dinitrobenzoate; methanesulfonyl chloride; With pyridine; In dichloromethane; at 0 - 20 ℃; for 1h;

With sodium hydrogencarbonate; In dichloromethane; water; for 0.5h;