2-bromo-3',4'-dihexyloxybenzophenone

Base Information

• Chemical Name: 2-bromo-3',4'-dihexyloxybenzophenone
• CAS No.: 220458-51-5
• Molecular Formula: C₂₅H₃₃BrO₃
• Molecular Weight: 461.439
• Mol file: 220458-51-5.mol

Synonyms:2-bromo-3',4'-dihexyloxybenzophenone

Chemical Property of 2-bromo-3',4'-dihexyloxybenzophenone

Chemical Property:

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Technology Process of 2-bromo-3',4'-dihexyloxybenzophenone

There total 1 articles about 2-bromo-3',4'-dihexyloxybenzophenone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

1,2-dihexyloxybenzene (94259-20-8) + 2-bromobenzoic acid chloride (7154-66-7) → 2-bromo-3',4'-dihexyloxybenzophenone (220458-51-5)

Guidance literature:

With aluminium trichloride; In dichloromethane; at 0 - 25 ℃; for 24h;

DOI:10.1021/jo9817523

Reference yield: 97.0%

2-bromo-3',4'-dihexyloxybenzophenone (220458-51-5) → cis-9,10-dihydroxy-9,10-bis(3,4-dihexyloxyphenyl)-9,10-dihydrophenanthrene

Guidance literature:

With [2,2]bipyridinyl; bis(1,5-cyclooctadiene)nickel ⁽⁰⁾; 1,5-cis,cis-cyclooctadiene; In N,N-dimethyl-formamide; at 20 - 60 ℃; for 3.3h;

DOI:10.1021/jo9817523

Reference yield: 93.0%

2-bromo-3',4'-dihexyloxybenzophenone (220458-51-5) → 10,10-bis(3,4-dihexyloxyphenyl)-9-phenanthrone

Guidance literature:

2-bromo-3',4'-dihexyloxybenzophenone; With [2,2]bipyridinyl; bis(1,5-cyclooctadiene)nickel ⁽⁰⁾; 1,5-cis,cis-cyclooctadiene; In N,N-dimethyl-formamide; at 20 - 60 ℃; for 3.3h;

Acid hydrolysis;

DOI:10.1021/jo9817523

upstream raw materials:

1,2-dihexyloxybenzene

2-bromobenzoic acid chloride