2-bromo-3',4'-dihexyloxybenzophenone

Base Information

Chemical Name:2-bromo-3',4'-dihexyloxybenzophenone
CAS No.:220458-51-5
Molecular Formula:C₂₅H₃₃BrO₃
Molecular Weight:461.439
Hs Code.:

Synonyms:2-bromo-3',4'-dihexyloxybenzophenone

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-bromo-3',4'-dihexyloxybenzophenone

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Technology Process of 2-bromo-3',4'-dihexyloxybenzophenone

There total 1 articles about 2-bromo-3',4'-dihexyloxybenzophenone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 94259-20-8
1,2-dihexyloxybenzene

: 7154-66-7
2-bromobenzoic acid chloride

: 220458-51-5
2-bromo-3',4'-dihexyloxybenzophenone

Guidance literature:: With aluminium trichloride; In dichloromethane; at 0 - 25 ℃; for 24h;
DOI:10.1021/jo9817523

Reference yield: 97.0%

: 220458-51-5
2-bromo-3',4'-dihexyloxybenzophenone

: cis-9,10-dihydroxy-9,10-bis(3,4-dihexyloxyphenyl)-9,10-dihydrophenanthrene

Guidance literature:: With [2,2]bipyridinyl; bis(1,5-cyclooctadiene)nickel ⁽⁰⁾; 1,5-cis,cis-cyclooctadiene; In N,N-dimethyl-formamide; at 20 - 60 ℃; for 3.3h;
DOI:10.1021/jo9817523

Reference yield: 93.0%

: 220458-51-5
2-bromo-3',4'-dihexyloxybenzophenone

: 10,10-bis(3,4-dihexyloxyphenyl)-9-phenanthrone

Guidance literature:: 2-bromo-3',4'-dihexyloxybenzophenone; With [2,2]bipyridinyl; bis(1,5-cyclooctadiene)nickel ⁽⁰⁾; 1,5-cis,cis-cyclooctadiene; In N,N-dimethyl-formamide; at 20 - 60 ℃; for 3.3h;

Acid hydrolysis;
DOI:10.1021/jo9817523