[Pd(η¹-3,3-Me2C3H3)(N,1-bis[2-(diphenylphosphino)phenyl]methanimine)]BF4

Base Information

• Chemical Name: [Pd(η¹-3,3-Me2C3H3)(N,1-bis[2-(diphenylphosphino)phenyl]methanimine)]BF4
• CAS No.: 1402556-68-6
• Molecular Formula: BF₄*C₄₂H₃₈NP₂Pd
• Molecular Weight: 811.943

Synonyms:[Pd(η¹-3,3-Me2C3H3)(N,1-bis[2-(diphenylphosphino)phenyl]methanimine)]BF4

Chemical Property of [Pd(η¹-3,3-Me2C3H3)(N,1-bis[2-(diphenylphosphino)phenyl]methanimine)]BF4

Chemical Property:

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Technology Process of [Pd(η¹-3,3-Me2C3H3)(N,1-bis[2-(diphenylphosphino)phenyl]methanimine)]BF4

There total 1 articles about [Pd(η¹-3,3-Me2C3H3)(N,1-bis[2-(diphenylphosphino)phenyl]methanimine)]BF4 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

sodium tetrafluoroborate (13755-29-8) + bis(μ-chloro)bis{(1,2,3-η)-3-methyl-2-butenyl}palladium (12288-41-4) + 2-(diphenylphosphino)-N-[2-(diphenylphosphino)benzylidene]benzeneamine (303745-38-2) → [Pd(η1-3,3-Me2C3H3)(N,1-bis[2-(diphenylphosphino)phenyl]methanimine)]BF4 (1402556-68-6)

Guidance literature:

In dichloromethane; at 20 ℃; for 2h; Inert atmosphere;

DOI:10.1039/c2dt30746d DOI:10.1039/c2dt30746d

Reference yield: 98.0%

piperidine (110-89-4) + [Pd(η1-3,3-Me2C3H3)(N,1-bis[2-(diphenylphosphino)phenyl]methanimine)]BF4 (1402556-68-6) + 1,2-Dicyanoethylene (764-42-1) → 1-(2-methylbutyl-3-en-2-yl)piperidine (223265-14-3) + [Pd(η2-fumaronitrile)(N,1-Bis[2-(diphenylphosphino)phenyl]methanimine)]·CH2Cl2

Guidance literature:

In chloroform-d1; at 24.84 ℃; for 12h; Inert atmosphere;

DOI:10.1039/c2dt30746d

Reference yield:

[Pd(η1-3,3-Me2C3H3)(N,1-bis[2-(diphenylphosphino)phenyl]methanimine)]BF4 (1402556-68-6) + diethylamine (109-89-7) + 1,2-Dicyanoethylene (764-42-1) → N,N-diethyl-3-methyl-2-butenylamine (10229-36-4) + 3-diethylamino-3-methyl-1-butene (60416-82-2) + [Pd(η2-fumaronitrile)(N,1-Bis[2-(diphenylphosphino)phenyl]methanimine)]·CH2Cl2

Guidance literature:

In chloroform-d1; at 24.84 ℃; Inert atmosphere;

DOI:10.1039/c2dt30746d

upstream raw materials:

sodium tetrafluoroborate

bis(μ-chloro)bis{(1,2,3-η)-3-methyl-2-butenyl}palladium

2-(diphenylphosphino)-N-[2-(diphenylphosphino)benzylidene]benzeneamine

Downstream raw materials:

N,N-diethyl-3-methyl-2-butenylamine

3-diethylamino-3-methyl-1-butene

1-(2-methylbutyl-3-en-2-yl)piperidine

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