N-[1-(1H-tetrazol-5-yl)-5,6,7,8-tetrahydronaphthalen-2-yl]-benzenesulfonamide

Base Information

Chemical Name:N-[1-(1H-tetrazol-5-yl)-5,6,7,8-tetrahydronaphthalen-2-yl]-benzenesulfonamide
CAS No.:1392091-22-3
Molecular Formula:C₁₇H₁₇N₅O₂S
Molecular Weight:355.42
Hs Code.:

Synonyms:N-[1-(1H-tetrazol-5-yl)-5,6,7,8-tetrahydronaphthalen-2-yl]-benzenesulfonamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-[1-(1H-tetrazol-5-yl)-5,6,7,8-tetrahydronaphthalen-2-yl]-benzenesulfonamide

Chemical Property:

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Technology Process of N-[1-(1H-tetrazol-5-yl)-5,6,7,8-tetrahydronaphthalen-2-yl]-benzenesulfonamide

There total 9 articles about N-[1-(1H-tetrazol-5-yl)-5,6,7,8-tetrahydronaphthalen-2-yl]-benzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1392091-32-5
N-(1-cyano-5,6,7,8-tetrahydronaphthalen-2-yl)benzenesulfonamide

: 1392091-22-3
N-[1-(1H-tetrazol-5-yl)-5,6,7,8-tetrahydronaphthalen-2-yl]-benzenesulfonamide

Guidance literature:: With sodium azide; tributyltin chloride; tetrabutylammomium bromide; In N,N-dimethyl-formamide; at 220 ℃; for 1h; Microwave irradiation;

Reference yield:

: 59604-96-5
2-hydroxy-5,6,7,8-tetrahydronaphthalene-1-carboxylic acid methyl ester

: 1392091-22-3
N-[1-(1H-tetrazol-5-yl)-5,6,7,8-tetrahydronaphthalen-2-yl]-benzenesulfonamide

Guidance literature:: Multi-step reaction with 8 steps

1.1: pyridine / dichloromethane / 1.58 h / -20 - 20 °C

2.1: caesium carbonate; triethylamine / palladium diacetate; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene / 1,4-dioxane / 3.5 h / 100 °C / Inert atmosphere

3.1: hydrogenchloride; water / tetrahydrofuran / 1 h

4.1: pyridine / 1 h

5.1: lithium hydroxide monohydrate; water / 1,4-dioxane / 0.25 h / 160 °C / Microwave irradiation

6.1: oxalyl dichloride; N,N-dimethyl-formamide / dichloromethane / 0.5 h

6.2: 1 h

7.1: phosphorus pentachloride / dichloromethane / 3 h

8.1: sodium azide; tributyltin chloride; tetrabutylammomium bromide / N,N-dimethyl-formamide / 1 h / 220 °C / Microwave irradiation

With pyridine; hydrogenchloride; sodium azide; oxalyl dichloride; lithium hydroxide monohydrate; phosphorus pentachloride; tributyltin chloride; tetrabutylammomium bromide; water; caesium carbonate; triethylamine; N,N-dimethyl-formamide; palladium diacetate; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; In tetrahydrofuran; 1,4-dioxane; dichloromethane; N,N-dimethyl-formamide;

Reference yield:

: 947-65-9
methyl 2-hydroxy-1-naphthoate

: 1392091-22-3
N-[1-(1H-tetrazol-5-yl)-5,6,7,8-tetrahydronaphthalen-2-yl]-benzenesulfonamide

Guidance literature:: Multi-step reaction with 9 steps

1.1: hydrogen; acetic acid / platinum(IV) oxide / 3000.3 Torr

2.1: pyridine / dichloromethane / 1.58 h / -20 - 20 °C

3.1: caesium carbonate; triethylamine / palladium diacetate; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene / 1,4-dioxane / 3.5 h / 100 °C / Inert atmosphere

4.1: hydrogenchloride; water / tetrahydrofuran / 1 h

5.1: pyridine / 1 h

6.1: lithium hydroxide monohydrate; water / 1,4-dioxane / 0.25 h / 160 °C / Microwave irradiation

7.1: oxalyl dichloride; N,N-dimethyl-formamide / dichloromethane / 0.5 h

7.2: 1 h

8.1: phosphorus pentachloride / dichloromethane / 3 h

9.1: sodium azide; tributyltin chloride; tetrabutylammomium bromide / N,N-dimethyl-formamide / 1 h / 220 °C / Microwave irradiation

With pyridine; hydrogenchloride; sodium azide; oxalyl dichloride; lithium hydroxide monohydrate; phosphorus pentachloride; tributyltin chloride; tetrabutylammomium bromide; water; hydrogen; caesium carbonate; acetic acid; triethylamine; N,N-dimethyl-formamide; platinum(IV) oxide; palladium diacetate; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; In tetrahydrofuran; 1,4-dioxane; dichloromethane; N,N-dimethyl-formamide;