(1S,2S,3S)-3-(4-bromophenyl)-2-fluoro-N-methoxy-N,2-dimethylcyclopropanecarboxamide

Base Information

Chemical Name:(1S,2S,3S)-3-(4-bromophenyl)-2-fluoro-N-methoxy-N,2-dimethylcyclopropanecarboxamide
CAS No.:1422177-03-4
Molecular Formula:C₁₃H₁₅BrFNO₂
Molecular Weight:316.17
Hs Code.:

Synonyms:(1S,2S,3S)-3-(4-bromophenyl)-2-fluoro-N-methoxy-N,2-dimethylcyclopropanecarboxamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (1S,2S,3S)-3-(4-bromophenyl)-2-fluoro-N-methoxy-N,2-dimethylcyclopropanecarboxamide

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Technology Process of (1S,2S,3S)-3-(4-bromophenyl)-2-fluoro-N-methoxy-N,2-dimethylcyclopropanecarboxamide

There total 2 articles about (1S,2S,3S)-3-(4-bromophenyl)-2-fluoro-N-methoxy-N,2-dimethylcyclopropanecarboxamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 1097193-00-4
N-((1-fluoroethyl)(oxo)(phenyl)-λ⁶-sulfaneylidene)-4-methylbenzenesulfonamide

: 652978-38-6
3-(4-bromophenyl)-N-methoxy-N-methylacrylamide

: 1422177-03-4
(1S,2S,3S)-3-(4-bromophenyl)-2-fluoro-N-methoxy-N,2-dimethylcyclopropanecarboxamide

Guidance literature:: With lithium hexamethyldisilazane; In tetrahydrofuran; at -78 - 25 ℃; for 3.33h; Inert atmosphere;

Reference yield:

: 652978-38-6
3-(4-bromophenyl)-N-methoxy-N-methylacrylamide

: 1422176-85-9
C₁₅H₁₆FNO₃S₂

: C₁₃H₁₅BrFNO₂

: 1422177-03-4
(1S,2S,3S)-3-(4-bromophenyl)-2-fluoro-N-methoxy-N,2-dimethylcyclopropanecarboxamide

: C₁₃H₁₅BrFNO₂

Guidance literature:: With lithium hexamethyldisilazane; In tetrahydrofuran; at -78 - 20 ℃; for 3.33333h; optical yield given as %ee; Inert atmosphere;
DOI:10.1002/anie.201202451