3-ethynyl-6-phenyl-4-(phenylethynyl)-1-(triisopropylsilyl)hex-3-ene-1,5-diyne

Base Information

• Chemical Name: 3-ethynyl-6-phenyl-4-(phenylethynyl)-1-(triisopropylsilyl)hex-3-ene-1,5-diyne
• CAS No.: 159461-31-1
• Molecular Formula: C₃₁H₃₂Si
• Molecular Weight: 432.681

Synonyms:3-ethynyl-6-phenyl-4-(phenylethynyl)-1-(triisopropylsilyl)hex-3-ene-1,5-diyne

Chemical Property of 3-ethynyl-6-phenyl-4-(phenylethynyl)-1-(triisopropylsilyl)hex-3-ene-1,5-diyne

Chemical Property:

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Technology Process of 3-ethynyl-6-phenyl-4-(phenylethynyl)-1-(triisopropylsilyl)hex-3-ene-1,5-diyne

There total 1 articles about 3-ethynyl-6-phenyl-4-(phenylethynyl)-1-(triisopropylsilyl)hex-3-ene-1,5-diyne which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 57.0%

1-phenyl-3-(phenylethynyl)-6-(triisopropylsilyl)-4-<(trimethylsilyl)ethynyl>hex-3-ene-1,5-diyne (167971-45-1) → 3-ethynyl-6-phenyl-4-(phenylethynyl)-1-(triisopropylsilyl)hex-3-ene-1,5-diyne (159461-31-1)

Guidance literature:

With potassium carbonate; In tetrahydrofuran; methanol; for 0.5h; Ambient temperature;

DOI:10.1002/hlca.19950780104

Reference yield: 72.0%

3-ethynyl-6-phenyl-4-(phenylethynyl)-1-(triisopropylsilyl)hex-3-ene-1,5-diyne (159461-31-1) → 4,9-bis<(triisopropylsilyl)ethynyl>-1,12-diphenyl-3,10-bis(phenylethynyl)dodeca-3,9-diene-1,5,7,11-tetrayne

Guidance literature:

With copper diacetate; In pyridine; benzene; Ambient temperature;

DOI:10.1002/hlca.19950780402

Reference yield: 57.0%

3-ethynyl-6-phenyl-4-(phenylethynyl)-1-(triisopropylsilyl)hex-3-ene-1,5-diyne (159461-31-1) + C26H22N2 (601488-61-3) → C88H82N2Si2 (601488-56-6)

Guidance literature:

With N,N,N,N,-tetramethylethylenediamine; oxygen; copper(l) chloride; In acetone; at 20 ℃; for 2h;

DOI:10.1039/b304130a

upstream raw materials:

1-phenyl-3-(phenylethynyl)-6-(triisopropylsilyl)-4-<(trimethylsilyl)ethynyl>hex-3-ene-1,5-diyne

Downstream raw materials:

C₈₈H₈₂N₂Si₂

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