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3-diphenylphosphinoisoquinolone

Base Information Edit
  • Chemical Name:3-diphenylphosphinoisoquinolone
  • CAS No.:851542-17-1
  • Molecular Formula:C21H16NOP
  • Molecular Weight:329.338
  • Hs Code.:
  • Mol file:851542-17-1.mol
3-diphenylphosphinoisoquinolone

Synonyms:3-diphenylphosphinoisoquinolone

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Chemical Property of 3-diphenylphosphinoisoquinolone Edit
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Technology Process of 3-diphenylphosphinoisoquinolone

There total 4 articles about 3-diphenylphosphinoisoquinolone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
triphenylphosphine; With ammonia; sodium; at -78 ℃; for 2h;
3-chloroisoquinolin-1(2H)-one; In tetrahydrofuran; at 60 ℃; for 20h;
Guidance literature:
3-bromo-1-tert-butoxyisoquinoline; With n-butyllithium; In tetrahydrofuran; at -100 ℃;
chloro-diphenylphosphine; at -100 - 20 ℃;
DOI:10.1002/anie.200462499
Guidance literature:
Multi-step reaction with 2 steps
1.1: toluene / 80 °C
2.1: nBuLi / tetrahydrofuran / -100 °C
2.2: -100 - 20 °C
With n-butyllithium; In tetrahydrofuran; toluene;
DOI:10.1002/anie.200462499
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