1-hydroxy-1-(chloroacetaminomethyl)-6,7-dibenzyloxy-1,2,3,4-tetrahydronaphthalene

Base Information

Chemical Name:1-hydroxy-1-(chloroacetaminomethyl)-6,7-dibenzyloxy-1,2,3,4-tetrahydronaphthalene
CAS No.:462100-15-8
Molecular Formula:C₂₇H₂₈ClNO₄
Molecular Weight:465.977
Hs Code.:

Synonyms:1-hydroxy-1-(chloroacetaminomethyl)-6,7-dibenzyloxy-1,2,3,4-tetrahydronaphthalene

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Chemical Property of 1-hydroxy-1-(chloroacetaminomethyl)-6,7-dibenzyloxy-1,2,3,4-tetrahydronaphthalene

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Technology Process of 1-hydroxy-1-(chloroacetaminomethyl)-6,7-dibenzyloxy-1,2,3,4-tetrahydronaphthalene

There total 1 articles about 1-hydroxy-1-(chloroacetaminomethyl)-6,7-dibenzyloxy-1,2,3,4-tetrahydronaphthalene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 79-04-9
chloroacetyl chloride

: 1-aminomethyl-6,7-bis-benzyloxy-1,2,3,4-tetrahydro-naphthalen-1-ol

: 462100-15-8
1-hydroxy-1-(chloroacetaminomethyl)-6,7-dibenzyloxy-1,2,3,4-tetrahydronaphthalene

Guidance literature:: With sodium hydroxide; In dichloromethane; water; at 20 ℃; for 2h;
DOI:10.1016/S0223-5234(01)01322-8

Reference yield: 80.0%

: 462100-15-8
1-hydroxy-1-(chloroacetaminomethyl)-6,7-dibenzyloxy-1,2,3,4-tetrahydronaphthalene

: 462100-17-0
C₂₇H₂₇NO₄

Guidance literature:: With potassium tert-butylate; In benzene; at 20 ℃; for 2.5h;
DOI:10.1016/S0223-5234(01)01322-8

Reference yield:

: 462100-15-8
1-hydroxy-1-(chloroacetaminomethyl)-6,7-dibenzyloxy-1,2,3,4-tetrahydronaphthalene

: 462100-20-5
C₂₇H₂₉NO₃

Guidance literature:: Multi-step reaction with 2 steps

1: 80 percent / KOt-Bu / benzene / 2.5 h / 20 °C

2: 90 percent / LiAlH₄ / tetrahydrofuran / 3 h / Heating

With lithium aluminium tetrahydride; potassium tert-butylate; In tetrahydrofuran; benzene;
DOI:10.1016/S0223-5234(01)01322-8