Technology Process of C25H24BrNO8
There total 6 articles about C25H24BrNO8 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
di-isopropyl azodicarboxylate; triphenylphosphine;
at 18 - 50 ℃;
for 15h;
DOI:10.1002/ejoc.201001133
- Guidance literature:
-
Multi-step reaction with 3 steps
1: tetrakis(triphenylphosphine) palladium(0); tetrabutylammomium bromide; potassium carbonate / tetrahydrofuran; water / 1 h / 60 °C / Inert atmosphere; Microwave irradiation
2: N-Bromosuccinimide / N,N-dimethyl-formamide / 16 h / 18 - 50 °C
3: di-isopropyl azodicarboxylate; triphenylphosphine / 15 h / 18 - 50 °C
With
N-Bromosuccinimide; tetrakis(triphenylphosphine) palladium(0); di-isopropyl azodicarboxylate; tetrabutylammomium bromide; potassium carbonate; triphenylphosphine;
In
tetrahydrofuran; water; N,N-dimethyl-formamide;
1: Suzuki coupling / 3: Mitsunobu reaction;
DOI:10.1002/ejoc.201001133
- Guidance literature:
-
Multi-step reaction with 2 steps
1: N-Bromosuccinimide / N,N-dimethyl-formamide / 16 h / 18 - 50 °C
2: di-isopropyl azodicarboxylate; triphenylphosphine / 15 h / 18 - 50 °C
With
N-Bromosuccinimide; di-isopropyl azodicarboxylate; triphenylphosphine;
In
N,N-dimethyl-formamide;
2: Mitsunobu reaction;
DOI:10.1002/ejoc.201001133