Technology Process of C29H30ClN3O5
There total 8 articles about C29H30ClN3O5 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
potassium carbonate;
In
N,N-dimethyl-formamide;
at 20 ℃;
for 2h;
Cooling with ice;
- Guidance literature:
-
Multi-step reaction with 7 steps
1: 0.5 h / -15 - 20 °C
2: lithium aluminium tetrahydride / tetrahydrofuran / 5 h / 20 °C / Cooling with ice
3: ammonium hydroxide; iodine / water; tetrahydrofuran / 3 h / 60 °C
4: triethylamine; hydroxylamine hydrochloride / methanol / 5 h / Reflux
5: triethylamine / dichloromethane / 0.5 h / 20 °C / Cooling with ice
6: 1,4-dioxane / 3 h / 100 °C
7: potassium carbonate / N,N-dimethyl-formamide / 2 h / 20 °C / Cooling with ice
With
ammonium hydroxide; lithium aluminium tetrahydride; hydroxylamine hydrochloride; iodine; potassium carbonate; triethylamine;
In
tetrahydrofuran; 1,4-dioxane; methanol; dichloromethane; water; N,N-dimethyl-formamide;
- Guidance literature:
-
Multi-step reaction with 5 steps
1: ammonium hydroxide; iodine / water; tetrahydrofuran / 3 h / 60 °C
2: triethylamine; hydroxylamine hydrochloride / methanol / 5 h / Reflux
3: triethylamine / dichloromethane / 0.5 h / 20 °C / Cooling with ice
4: 1,4-dioxane / 3 h / 100 °C
5: potassium carbonate / N,N-dimethyl-formamide / 2 h / 20 °C / Cooling with ice
With
ammonium hydroxide; hydroxylamine hydrochloride; iodine; potassium carbonate; triethylamine;
In
tetrahydrofuran; 1,4-dioxane; methanol; dichloromethane; water; N,N-dimethyl-formamide;