2,2'-(4-fluoro-1,2-phenylene)bisoxydiethanol

Base Information

• Chemical Name: 2,2'-(4-fluoro-1,2-phenylene)bisoxydiethanol
• CAS No.: 1260398-02-4
• Molecular Formula: C₁₀H₁₃FO₄
• Molecular Weight: 216.209
• Mol file: 1260398-02-4.mol

Synonyms:2,2'-(4-fluoro-1,2-phenylene)bisoxydiethanol

Chemical Property of 2,2'-(4-fluoro-1,2-phenylene)bisoxydiethanol

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2,2'-(4-fluoro-1,2-phenylene)bisoxydiethanol

There total 1 articles about 2,2'-(4-fluoro-1,2-phenylene)bisoxydiethanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

4-fluoropyrocatechol (367-32-8) + 2-chloro-ethanol (107-07-3) → 2,2'-(4-fluoro-1,2-phenylene)bisoxydiethanol (1260398-02-4)

Guidance literature:

4-fluoropyrocatechol; With sodium hydroxide; In water; butan-1-ol; for 0.0833333h; Inert atmosphere; Reflux;

2-chloro-ethanol; In water; butan-1-ol; for 19h; Inert atmosphere; Reflux;

DOI:10.1002/anie.201002789

Reference yield: 77.0%

2,2'-(4-fluoro-1,2-phenylene)bisoxydiethanol (1260398-02-4) + p-toluenesulfonyl chloride (98-59-9) → 2,2'-(4-fluoro-1,2-phenylene)bisoxybis(ethane-2,1-diyl)bis(4-methylbenzenesulfonate) (1260398-03-5)

Guidance literature:

With triethylamine; In dichloromethane; at 0 - 20 ℃; Inert atmosphere;

DOI:10.1002/anie.201002789

upstream raw materials:

4-fluoropyrocatechol

2-chloro-ethanol

Downstream raw materials:

2,2'-(4-fluoro-1,2-phenylene)bisoxybis(ethane-2,1-diyl)bis(4-methylbenzenesulfonate)