1-(benzyloxy)-4(R )-(1-(4-(benzyloxy)-3-methoxyphenyl)-2-nitroethyl)benzene

Base Information

Chemical Name:1-(benzyloxy)-4(R )-(1-(4-(benzyloxy)-3-methoxyphenyl)-2-nitroethyl)benzene
CAS No.:1306747-17-0
Molecular Formula:C₂₉H₂₇NO₅
Molecular Weight:469.537
Hs Code.:

Synonyms:1-(benzyloxy)-4(R )-(1-(4-(benzyloxy)-3-methoxyphenyl)-2-nitroethyl)benzene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-(benzyloxy)-4(R )-(1-(4-(benzyloxy)-3-methoxyphenyl)-2-nitroethyl)benzene

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Technology Process of 1-(benzyloxy)-4(R )-(1-(4-(benzyloxy)-3-methoxyphenyl)-2-nitroethyl)benzene

There total 1 articles about 1-(benzyloxy)-4(R )-(1-(4-(benzyloxy)-3-methoxyphenyl)-2-nitroethyl)benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 63909-38-6,1860-56-6
3-methoxy-4-benzyloxy-ω-nitrostyrolene

: 146631-00-7
[4-(benzyloxy)phenyl]boronic acid

: 1306747-17-0
1-(benzyloxy)-4(R )-(1-(4-(benzyloxy)-3-methoxyphenyl)-2-nitroethyl)benzene

Guidance literature:: With chlorobis(ethylene)rhodium(I) dimer; tert-butanesulfinylphosphine; triethylamine; In ethanol; at 40 ℃; for 10h; optical yield given as %ee; enantioselective reaction; Inert atmosphere;
DOI:10.1002/chem.201100135

Reference yield:

: 1306747-17-0
1-(benzyloxy)-4(R )-(1-(4-(benzyloxy)-3-methoxyphenyl)-2-nitroethyl)benzene

: C₂₉H₂₉NO₃

Guidance literature:: With sodium tetrahydroborate; nickel(II) chloride hexahydrate; In methanol; chloroform; at 0 ℃;
DOI:10.1002/chem.201100135

Reference yield:

: 1306747-17-0
1-(benzyloxy)-4(R )-(1-(4-(benzyloxy)-3-methoxyphenyl)-2-nitroethyl)benzene

: (4R)-4-(4-hydroxyphenyl)-6-methoxy-2-methyl-1,2,3,4-tetrahydroisoquinolin-7-ol

Guidance literature:: Multi-step reaction with 3 steps

1: sodium tetrahydroborate; nickel(II) chloride hexahydrate / methanol; chloroform / 0 °C

2: 6 h / 100 °C / Inert atmosphere

3: hydrogenchloride; water / ethanol / 4 h / Inert atmosphere; Reflux

With hydrogenchloride; sodium tetrahydroborate; nickel(II) chloride hexahydrate; water; In methanol; ethanol; chloroform;
DOI:10.1002/chem.201100135