(R)-7-(benzyloxy)-4-(4-(benzyloxy)phenyl)-1,2,3,4-tetrahydro-6-methoxy-2-methyl isoquinoline

Base Information

Chemical Name:(R)-7-(benzyloxy)-4-(4-(benzyloxy)phenyl)-1,2,3,4-tetrahydro-6-methoxy-2-methyl isoquinoline
CAS No.:1306747-18-1
Molecular Formula:C₃₁H₃₁NO₃
Molecular Weight:465.592
Hs Code.:

Synonyms:(R)-7-(benzyloxy)-4-(4-(benzyloxy)phenyl)-1,2,3,4-tetrahydro-6-methoxy-2-methyl isoquinoline

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Chemical Property of (R)-7-(benzyloxy)-4-(4-(benzyloxy)phenyl)-1,2,3,4-tetrahydro-6-methoxy-2-methyl isoquinoline

Chemical Property:

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Technology Process of (R)-7-(benzyloxy)-4-(4-(benzyloxy)phenyl)-1,2,3,4-tetrahydro-6-methoxy-2-methyl isoquinoline

There total 4 articles about (R)-7-(benzyloxy)-4-(4-(benzyloxy)phenyl)-1,2,3,4-tetrahydro-6-methoxy-2-methyl isoquinoline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 63909-38-6,1860-56-6
3-methoxy-4-benzyloxy-ω-nitrostyrolene

: 1306747-18-1
(R)-7-(benzyloxy)-4-(4-(benzyloxy)phenyl)-1,2,3,4-tetrahydro-6-methoxy-2-methyl isoquinoline

Guidance literature:: Multi-step reaction with 3 steps

1: chlorobis(ethylene)rhodium(I) dimer; tert-butanesulfinylphosphine; triethylamine / ethanol / 10 h / 40 °C / Inert atmosphere

2: sodium tetrahydroborate; nickel(II) chloride hexahydrate / methanol; chloroform / 0 °C

3: 6 h / 100 °C / Inert atmosphere

With sodium tetrahydroborate; chlorobis(ethylene)rhodium(I) dimer; nickel(II) chloride hexahydrate; tert-butanesulfinylphosphine; triethylamine; In methanol; ethanol; chloroform;
DOI:10.1002/chem.201100135

Reference yield:

: 146631-00-7
[4-(benzyloxy)phenyl]boronic acid

: 1306747-18-1
(R)-7-(benzyloxy)-4-(4-(benzyloxy)phenyl)-1,2,3,4-tetrahydro-6-methoxy-2-methyl isoquinoline

Guidance literature:: Multi-step reaction with 3 steps

1: chlorobis(ethylene)rhodium(I) dimer; tert-butanesulfinylphosphine; triethylamine / ethanol / 10 h / 40 °C / Inert atmosphere

2: sodium tetrahydroborate; nickel(II) chloride hexahydrate / methanol; chloroform / 0 °C

3: 6 h / 100 °C / Inert atmosphere

With sodium tetrahydroborate; chlorobis(ethylene)rhodium(I) dimer; nickel(II) chloride hexahydrate; tert-butanesulfinylphosphine; triethylamine; In methanol; ethanol; chloroform;
DOI:10.1002/chem.201100135

Reference yield:

: 1306747-17-0
1-(benzyloxy)-4(R )-(1-(4-(benzyloxy)-3-methoxyphenyl)-2-nitroethyl)benzene

: 1306747-18-1
(R)-7-(benzyloxy)-4-(4-(benzyloxy)phenyl)-1,2,3,4-tetrahydro-6-methoxy-2-methyl isoquinoline

Guidance literature:: Multi-step reaction with 2 steps

1: sodium tetrahydroborate; nickel(II) chloride hexahydrate / methanol; chloroform / 0 °C

2: 6 h / 100 °C / Inert atmosphere

With sodium tetrahydroborate; nickel(II) chloride hexahydrate; In methanol; chloroform;
DOI:10.1002/chem.201100135