(2Z,2'Z)-3,3'-(((1E,1'E)-(2-cyclohexyl-1,3-dioxoisoindoline-4,7-diyl)bis(ethene-2,1-diyl))bis(4,1-phenylene))bis(2-(4-nitrophenyl)acrylonitrile)

Base Information

Chemical Name:(2Z,2'Z)-3,3'-(((1E,1'E)-(2-cyclohexyl-1,3-dioxoisoindoline-4,7-diyl)bis(ethene-2,1-diyl))bis(4,1-phenylene))bis(2-(4-nitrophenyl)acrylonitrile)
CAS No.:1387566-54-2
Molecular Formula:C₄₈H₃₅N₅O₆
Molecular Weight:777.836
Hs Code.:

Synonyms:(2Z,2'Z)-3,3'-(((1E,1'E)-(2-cyclohexyl-1,3-dioxoisoindoline-4,7-diyl)bis(ethene-2,1-diyl))bis(4,1-phenylene))bis(2-(4-nitrophenyl)acrylonitrile)

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Chemical Property of (2Z,2'Z)-3,3'-(((1E,1'E)-(2-cyclohexyl-1,3-dioxoisoindoline-4,7-diyl)bis(ethene-2,1-diyl))bis(4,1-phenylene))bis(2-(4-nitrophenyl)acrylonitrile)

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Technology Process of (2Z,2'Z)-3,3'-(((1E,1'E)-(2-cyclohexyl-1,3-dioxoisoindoline-4,7-diyl)bis(ethene-2,1-diyl))bis(4,1-phenylene))bis(2-(4-nitrophenyl)acrylonitrile)

There total 6 articles about (2Z,2'Z)-3,3'-(((1E,1'E)-(2-cyclohexyl-1,3-dioxoisoindoline-4,7-diyl)bis(ethene-2,1-diyl))bis(4,1-phenylene))bis(2-(4-nitrophenyl)acrylonitrile) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

: 1387566-56-4
4,4'-((1E,1'E)-(2-cyclohexyl-1,3-dioxoisoindoline-4,7-diyl)bis(ethene-2,1-diyl))dibenzaldehyde

: 555-21-5,34512-13-5,174848-08-9
4-Nitrophenylacetonitrile

: 1387566-54-2
(2Z,2'Z)-3,3'-(((1E,1'E)-(2-cyclohexyl-1,3-dioxoisoindoline-4,7-diyl)bis(ethene-2,1-diyl))bis(4,1-phenylene))bis(2-(4-nitrophenyl)acrylonitrile)

Guidance literature:: With sodium hydroxide; In ethanol; N,N-dimethyl-formamide; at 20 ℃; Inert atmosphere;
DOI:10.1039/c2jm16915k

Reference yield:

: 85-44-9
phthalic anhydride

: 1387566-54-2
(2Z,2'Z)-3,3'-(((1E,1'E)-(2-cyclohexyl-1,3-dioxoisoindoline-4,7-diyl)bis(ethene-2,1-diyl))bis(4,1-phenylene))bis(2-(4-nitrophenyl)acrylonitrile)

Guidance literature:: Multi-step reaction with 4 steps

1: sulfuric acid; bromine

2: acetic acid / 5 h / Reflux

3: palladium diacetate; triethylamine; tris-(o-tolyl)phosphine / N,N-dimethyl-formamide / 24 h / 90 °C / Inert atmosphere

4: sodium hydroxide / ethanol; N,N-dimethyl-formamide / 20 °C / Inert atmosphere

With sulfuric acid; bromine; palladium diacetate; acetic acid; triethylamine; tris-(o-tolyl)phosphine; sodium hydroxide; In ethanol; N,N-dimethyl-formamide;
DOI:10.1039/c2jm16915k

Reference yield:

: 25834-16-6
4,7-dibromoisobenzofuran-1,3-dione

: 1387566-54-2
(2Z,2'Z)-3,3'-(((1E,1'E)-(2-cyclohexyl-1,3-dioxoisoindoline-4,7-diyl)bis(ethene-2,1-diyl))bis(4,1-phenylene))bis(2-(4-nitrophenyl)acrylonitrile)

Guidance literature:: Multi-step reaction with 3 steps

1: acetic acid / 5 h / Reflux

2: palladium diacetate; triethylamine; tris-(o-tolyl)phosphine / N,N-dimethyl-formamide / 24 h / 90 °C / Inert atmosphere

3: sodium hydroxide / ethanol; N,N-dimethyl-formamide / 20 °C / Inert atmosphere

With palladium diacetate; acetic acid; triethylamine; tris-(o-tolyl)phosphine; sodium hydroxide; In ethanol; N,N-dimethyl-formamide;
DOI:10.1039/c2jm16915k