4,4'-((1E,1'E)-(2-cyclohexyl-1,3-dioxoisoindoline-4,7-diyl)bis(ethene-2,1-diyl))dibenzaldehyde

Base Information

Chemical Name:4,4'-((1E,1'E)-(2-cyclohexyl-1,3-dioxoisoindoline-4,7-diyl)bis(ethene-2,1-diyl))dibenzaldehyde
CAS No.:1387566-56-4
Molecular Formula:C₃₂H₂₇NO₄
Molecular Weight:489.571
Hs Code.:

Synonyms:4,4'-((1E,1'E)-(2-cyclohexyl-1,3-dioxoisoindoline-4,7-diyl)bis(ethene-2,1-diyl))dibenzaldehyde

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Chemical Property of 4,4'-((1E,1'E)-(2-cyclohexyl-1,3-dioxoisoindoline-4,7-diyl)bis(ethene-2,1-diyl))dibenzaldehyde

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Technology Process of 4,4'-((1E,1'E)-(2-cyclohexyl-1,3-dioxoisoindoline-4,7-diyl)bis(ethene-2,1-diyl))dibenzaldehyde

There total 4 articles about 4,4'-((1E,1'E)-(2-cyclohexyl-1,3-dioxoisoindoline-4,7-diyl)bis(ethene-2,1-diyl))dibenzaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 56.0%

: 1791-26-0
4-vinyl-benzaldehyde

: 1387566-55-3
4,7-dibromo-2-cyclohexylisoindoline-1,3-dione

: 1387566-56-4
4,4'-((1E,1'E)-(2-cyclohexyl-1,3-dioxoisoindoline-4,7-diyl)bis(ethene-2,1-diyl))dibenzaldehyde

Guidance literature:: With palladium diacetate; triethylamine; tris-(o-tolyl)phosphine; In N,N-dimethyl-formamide; at 90 ℃; for 24h; Inert atmosphere;
DOI:10.1039/c2jm16915k

Reference yield:

: 85-44-9
phthalic anhydride

: 1387566-56-4
4,4'-((1E,1'E)-(2-cyclohexyl-1,3-dioxoisoindoline-4,7-diyl)bis(ethene-2,1-diyl))dibenzaldehyde

Guidance literature:: Multi-step reaction with 3 steps

1: sulfuric acid; bromine

2: acetic acid / 5 h / Reflux

3: palladium diacetate; triethylamine; tris-(o-tolyl)phosphine / N,N-dimethyl-formamide / 24 h / 90 °C / Inert atmosphere

With sulfuric acid; bromine; palladium diacetate; acetic acid; triethylamine; tris-(o-tolyl)phosphine; In N,N-dimethyl-formamide;
DOI:10.1039/c2jm16915k

Reference yield:

: 25834-16-6
4,7-dibromoisobenzofuran-1,3-dione

: 1387566-56-4
4,4'-((1E,1'E)-(2-cyclohexyl-1,3-dioxoisoindoline-4,7-diyl)bis(ethene-2,1-diyl))dibenzaldehyde

Guidance literature:: Multi-step reaction with 2 steps

1: acetic acid / 5 h / Reflux

2: palladium diacetate; triethylamine; tris-(o-tolyl)phosphine / N,N-dimethyl-formamide / 24 h / 90 °C / Inert atmosphere

With palladium diacetate; acetic acid; triethylamine; tris-(o-tolyl)phosphine; In N,N-dimethyl-formamide;
DOI:10.1039/c2jm16915k