Technology Process of 4,4'-((1E,1'E)-(2-cyclohexyl-1,3-dioxoisoindoline-4,7-diyl)bis(ethene-2,1-diyl))dibenzaldehyde
There total 4 articles about 4,4'-((1E,1'E)-(2-cyclohexyl-1,3-dioxoisoindoline-4,7-diyl)bis(ethene-2,1-diyl))dibenzaldehyde which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
palladium diacetate; triethylamine; tris-(o-tolyl)phosphine;
In
N,N-dimethyl-formamide;
at 90 ℃;
for 24h;
Inert atmosphere;
DOI:10.1039/c2jm16915k
- Guidance literature:
-
Multi-step reaction with 3 steps
1: sulfuric acid; bromine
2: acetic acid / 5 h / Reflux
3: palladium diacetate; triethylamine; tris-(o-tolyl)phosphine / N,N-dimethyl-formamide / 24 h / 90 °C / Inert atmosphere
With
sulfuric acid; bromine; palladium diacetate; acetic acid; triethylamine; tris-(o-tolyl)phosphine;
In
N,N-dimethyl-formamide;
DOI:10.1039/c2jm16915k
- Guidance literature:
-
Multi-step reaction with 2 steps
1: acetic acid / 5 h / Reflux
2: palladium diacetate; triethylamine; tris-(o-tolyl)phosphine / N,N-dimethyl-formamide / 24 h / 90 °C / Inert atmosphere
With
palladium diacetate; acetic acid; triethylamine; tris-(o-tolyl)phosphine;
In
N,N-dimethyl-formamide;
DOI:10.1039/c2jm16915k
