(1α,2α,3α,4α,5α,6α,7α,8α)-3,8-Bis(phenylsulfonyl)tricyclo<5.1.0.0^2,4>octan-5,6-diol-bis(benzolsulfonat)

Base Information

• Chemical Name: (1α,2α,3α,4α,5α,6α,7α,8α)-3,8-Bis(phenylsulfonyl)tricyclo<5.1.0.0^2,4>octan-5,6-diol-bis(benzolsulfonat)
• CAS No.: 96362-82-2
• Molecular Formula: C₃₂H₂₈O₁₀S₄
• Molecular Weight: 700.832

Synonyms:(1α,2α,3α,4α,5α,6α,7α,8α)-3,8-Bis(phenylsulfonyl)tricyclo<5.1.0.0^2,4>octan-5,6-diol-bis(benzolsulfonat)

Chemical Property of (1α,2α,3α,4α,5α,6α,7α,8α)-3,8-Bis(phenylsulfonyl)tricyclo<5.1.0.0^2,4>octan-5,6-diol-bis(benzolsulfonat)

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of (1α,2α,3α,4α,5α,6α,7α,8α)-3,8-Bis(phenylsulfonyl)tricyclo<5.1.0.0^2,4>octan-5,6-diol-bis(benzolsulfonat)

There total 11 articles about (1α,2α,3α,4α,5α,6α,7α,8α)-3,8-Bis(phenylsulfonyl)tricyclo<5.1.0.0^2,4>octan-5,6-diol-bis(benzolsulfonat) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

(1α,2α,3α,4α,5α,6α,7α,8α)-3,8-Bis(phenylsulfonyl)tricyclo<5.1.0.02,4>octan-5,6-diol (96362-80-0) + benzenesulfonyl chloride (98-09-9) → (1α,2α,3α,4α,5α,6α,7α,8α)-3,8-Bis(phenylsulfonyl)tricyclo<5.1.0.02,4>octan-5,6-diol-bis(benzolsulfonat) (96362-82-2)

Guidance literature:

With dmap; triethylamine; In pyridine; dichloromethane; for 12h;

Reference yield: 90.0%

(1α,2α,3α,4α,5α,6α,7α,8α)-5,6-O-Isopropyliden-3,8-bis(phenylsulfonyl)tricyclo<5.1.0.02,4>octan-5,6-diol (96362-81-1) → (1α,2α,3α,4α,5α,6α,7α,8α)-3,8-Bis(phenylsulfonyl)tricyclo<5.1.0.02,4>octan-5,6-diol-bis(benzolsulfonat) (96362-82-2)

Guidance literature:

Reference yield:

(1α,2α,3α,4β,5α,6α,7α)-(+/-)-2,3-O-Isopropyliden-7-(phenylsulfonyl)-4-(phenylsulfonylmethyl)bicyclo<4.1.o>heptan-2,3,5-triol (109583-84-8) → (1α,2α,3α,4α,5α,6α,7α,8α)-3,8-Bis(phenylsulfonyl)tricyclo<5.1.0.02,4>octan-5,6-diol-bis(benzolsulfonat) (96362-82-2)

Guidance literature:

Multi-step reaction with 4 steps

1: 88 percent / NEt₃ / CH₂Cl₂ / 0.5 h / 20 °C

2: 85 percent / 2.0M n-BuLi, diisopropylamine / hexane; tetrahydrofuran / 0.08 h / -20 °C

3: 91 percent / conc. HCl / methanol / 0.17 h / Heating

4: 91 percent / NEt₃, 4-(dimethylamino)pyridine / CH₂Cl₂; pyridine / 12 h

With hydrogenchloride; dmap; n-butyllithium; triethylamine; diisopropylamine; In tetrahydrofuran; pyridine; methanol; hexane; dichloromethane;

upstream raw materials:

cis-trisoxirane

(1α,2α,3α,4α,5α,6α,7α,8α)-3,8-Bis(phenylsulfonyl)tricyclo<5.1.0.0^2,4>octan-5,6-diol

benzenesulfonyl chloride

(1α,2α,3α,4α,5α,6α,7α,8α)-5,6-O-Isopropyliden-3,8-bis(phenylsulfonyl)tricyclo<5.1.0.0^2,4>octan-5,6-diol

Downstream raw materials:

(3α,4α,5α,7α)-(+/-)-1,4-Bis(phenylsulfonyl)tetracyclo<4.2.0.0^2,8.0^3,5>octan-7-ol

(1α,6α,7α,8α)-(+/-)-3,8-Bis(phenylsulfonyl)tetracyclo<5.1.8.0^2,4.0^3,5>octan-6-ol-benzolsulfonat

(Z)-3,7-Bis(phenylsulfonyl)pentacyclo<5.1.0.0^2,4.0^3,5.0^6,8>octan

4,5-Bis(phenylsulfonyl)tetracyclo<3.3.0.0^2,4.0^3.6>oct-7-en

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