tert-butyl({(1R,2R,4R,6R)-1-methyl-4-[(triethylsilyl)oxy]-7-oxabicyclo[4.1.0]hept-2-yl}oxy)diphenylsilane

Base Information

Chemical Name:tert-butyl({(1R,2R,4R,6R)-1-methyl-4-[(triethylsilyl)oxy]-7-oxabicyclo[4.1.0]hept-2-yl}oxy)diphenylsilane
CAS No.:1154607-02-9
Molecular Formula:C₂₉H₄₄O₃Si₂
Molecular Weight:496.838
Hs Code.:

Synonyms:tert-butyl({(1R,2R,4R,6R)-1-methyl-4-[(triethylsilyl)oxy]-7-oxabicyclo[4.1.0]hept-2-yl}oxy)diphenylsilane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of tert-butyl({(1R,2R,4R,6R)-1-methyl-4-[(triethylsilyl)oxy]-7-oxabicyclo[4.1.0]hept-2-yl}oxy)diphenylsilane

Chemical Property:

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Technology Process of tert-butyl({(1R,2R,4R,6R)-1-methyl-4-[(triethylsilyl)oxy]-7-oxabicyclo[4.1.0]hept-2-yl}oxy)diphenylsilane

There total 1 articles about tert-butyl({(1R,2R,4R,6R)-1-methyl-4-[(triethylsilyl)oxy]-7-oxabicyclo[4.1.0]hept-2-yl}oxy)diphenylsilane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 994-30-9
triethylsilyl chloride

: 1154606-96-8
(1R,3R,5R,6R)-5-{[tert-butyl(diphenyl)silyl]oxy}-6-methyl-7-oxabicyclo[4.1.0]heptan-3-ol

: 1154607-02-9
tert-butyl({(1R,2R,4R,6R)-1-methyl-4-[(triethylsilyl)oxy]-7-oxabicyclo[4.1.0]hept-2-yl}oxy)diphenylsilane

Guidance literature:: With 1H-imidazole; In N,N-dimethyl-formamide; at 20 ℃;

Reference yield:

: 1154607-02-9
tert-butyl({(1R,2R,4R,6R)-1-methyl-4-[(triethylsilyl)oxy]-7-oxabicyclo[4.1.0]hept-2-yl}oxy)diphenylsilane

: 1154607-03-0
(1R,3R,5R)-3-{[tert-butyl(diphenyl)silyl]oxy}-2-methylene-5-[(triethylsilyl)oxy]cyclohexanol

Guidance literature:: With 2,2,6,6-tetramethyl-piperidine; n-butyllithium; diethyl aluminiumcholoride; In hexane; toluene; at 0 - 20 ℃; for 3h;