4-nitro-4-phenylheptanedinitrile

Base Information

• Chemical Name: 4-nitro-4-phenylheptanedinitrile
• CAS No.: 10524-19-3
• Molecular Formula: C₁₃H₁₃N₃O₂
• Molecular Weight: 243.265

Synonyms:4-nitro-4-phenylheptanedinitrile

Chemical Property of 4-nitro-4-phenylheptanedinitrile

Chemical Property:

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Technology Process of 4-nitro-4-phenylheptanedinitrile

There total 1 articles about 4-nitro-4-phenylheptanedinitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

1-nitro-1-phenylmethane (622-42-4) + acrylonitrile (107-13-1,25014-41-9) → 4-nitro-4-phenylheptanedinitrile (10524-19-3)

Guidance literature:

With potassium fluoride; 18-crown-6 ether; In dichloromethane; at 20 ℃; for 72h;

DOI:10.1002/chem.202100890

Reference yield: 95.0%

4-nitro-4-phenylheptanedinitrile (10524-19-3) → 4-phenylheptanedinitrile (833-55-6)

Guidance literature:

With 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; In benzene; for 23h; Reflux;

DOI:10.1002/chem.202100890

upstream raw materials:

1-nitro-1-phenylmethane

acrylonitrile

Downstream raw materials:

4-phenylheptanedinitrile

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