Technology Process of C19H12ClFN2O2Se
There total 7 articles about C19H12ClFN2O2Se which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
sodium carbonate;
tetrakis(triphenylphosphine) palladium(0);
In
1,2-dimethoxyethane; ethanol; water;
at 110 ℃;
for 0.5h;
Inert atmosphere;
Microwave irradiation;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: boron tribromide / dichloromethane / 2 h / 20 °C
2.1: ytterbium(III) triflate / ethanol / 1 h / 90 °C
3.1: potassium acetate / dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH2Cl2 / 1,4-dioxane / 20 h / 90 °C / Inert atmosphere
3.2: 0.5 h / 20 °C
4.1: sodium carbonate / tetrakis(triphenylphosphine) palladium(0) / 1,2-dimethoxyethane; ethanol; water / 0.5 h / 110 °C / Inert atmosphere; Microwave irradiation
With
potassium acetate; boron tribromide; sodium carbonate;
tetrakis(triphenylphosphine) palladium(0); dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH2Cl2; ytterbium(III) triflate;
In
1,4-dioxane; 1,2-dimethoxyethane; ethanol; dichloromethane; water;
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: potassium acetate / dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH2Cl2 / 1,4-dioxane / 20 h / 90 °C / Inert atmosphere
1.2: 0.5 h / 20 °C
2.1: sodium carbonate / tetrakis(triphenylphosphine) palladium(0) / 1,2-dimethoxyethane; ethanol; water / 0.5 h / 110 °C / Inert atmosphere; Microwave irradiation
With
potassium acetate; sodium carbonate;
tetrakis(triphenylphosphine) palladium(0); dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH2Cl2;
In
1,4-dioxane; 1,2-dimethoxyethane; ethanol; water;