2-(4-methyl-1,2,3-thiadiazole-5-carbonyl)-N-phenylhydrazinecarbothioamide

Base Information

• Chemical Name: 2-(4-methyl-1,2,3-thiadiazole-5-carbonyl)-N-phenylhydrazinecarbothioamide
• CAS No.: 1260230-34-9
• Molecular Formula: C₁₁H₁₁N₅OS₂
• Molecular Weight: 293.373

Synonyms:2-(4-methyl-1,2,3-thiadiazole-5-carbonyl)-N-phenylhydrazinecarbothioamide

Chemical Property of 2-(4-methyl-1,2,3-thiadiazole-5-carbonyl)-N-phenylhydrazinecarbothioamide

Chemical Property:

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Technology Process of 2-(4-methyl-1,2,3-thiadiazole-5-carbonyl)-N-phenylhydrazinecarbothioamide

There total 1 articles about 2-(4-methyl-1,2,3-thiadiazole-5-carbonyl)-N-phenylhydrazinecarbothioamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

phenyl isothiocyanate (103-72-0) + 4-methyl-4,5-dihydro-1,2,3-thiadiazole-5-carbohydrazide (75423-15-3) → 2-(4-methyl-1,2,3-thiadiazole-5-carbonyl)-N-phenylhydrazinecarbothioamide (1260230-34-9)

Guidance literature:

In diethyl ether; at 20 ℃; for 336h;

DOI:10.1002/hc.20643

Reference yield: 74.0%

2-(4-methyl-1,2,3-thiadiazole-5-carbonyl)-N-phenylhydrazinecarbothioamide (1260230-34-9) → 2-(phenylamino)-5-(4-methyl-1,2,3-thiadiazol-5-yl)-1,3,4-thiadiazole (1260230-45-2)

Guidance literature:

With sulfuric acid; at 20 ℃; for 4h;

DOI:10.1002/hc.20643

Reference yield:

2-(4-methyl-1,2,3-thiadiazole-5-carbonyl)-N-phenylhydrazinecarbothioamide (1260230-34-9) → 5-(4-methyl-1,2,3-thiadiazol-5-yl)-4-phenyl-4H-1,2,4-triazole-3-thiol (1260230-40-7)

Guidance literature:

With sodium hydroxide; In water; for 4h; Reflux;

DOI:10.3390/molecules181012725

upstream raw materials:

phenyl isothiocyanate

4-methyl-4,5-dihydro-1,2,3-thiadiazole-5-carbohydrazide

Downstream raw materials:

4-phenyl-5-(4-methyl-1,2,3-thiadiazol-5-yl)-s-triazole-3-thione

2-(phenylamino)-5-(4-methyl-1,2,3-thiadiazol-5-yl)-1,3,4-thiadiazole

5-(4-methyl-1,2,3-thiadiazol-5-yl)-4-phenyl-4H-1,2,4-triazole-3-thiol

5-(5-((2,4-dichlorobenzyl)thio)-4-phenyl-4H-1,2,4-triazol-3-yl)-4-methyl-1,2,3-thiadiazole

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