3,6-dihydro-4-methyl-6-(3-nitrophenyl)-2-oxo-1,5-pyrimidinedicarboxylic acid 1-(1,1-dimethylethyl) 5-ethyl diester

Base Information

Chemical Name:3,6-dihydro-4-methyl-6-(3-nitrophenyl)-2-oxo-1,5-pyrimidinedicarboxylic acid 1-(1,1-dimethylethyl) 5-ethyl diester
CAS No.:108930-65-0
Molecular Formula:C₁₉H₂₃N₃O₇
Molecular Weight:405.408
Hs Code.:

Synonyms:3,6-dihydro-4-methyl-6-(3-nitrophenyl)-2-oxo-1,5-pyrimidinedicarboxylic acid 1-(1,1-dimethylethyl) 5-ethyl diester

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Chemical Property of 3,6-dihydro-4-methyl-6-(3-nitrophenyl)-2-oxo-1,5-pyrimidinedicarboxylic acid 1-(1,1-dimethylethyl) 5-ethyl diester

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Technology Process of 3,6-dihydro-4-methyl-6-(3-nitrophenyl)-2-oxo-1,5-pyrimidinedicarboxylic acid 1-(1,1-dimethylethyl) 5-ethyl diester

There total 5 articles about 3,6-dihydro-4-methyl-6-(3-nitrophenyl)-2-oxo-1,5-pyrimidinedicarboxylic acid 1-(1,1-dimethylethyl) 5-ethyl diester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: 106720-60-9
1,4-dihydro-2-methoxy-6-methyl-4-(3-nitrophenyl)-5-pyrimidinecarboxylic acid ethyl ester

: 108930-65-0
3,6-dihydro-4-methyl-6-(3-nitrophenyl)-2-oxo-1,5-pyrimidinedicarboxylic acid 1-(1,1-dimethylethyl) 5-ethyl diester

Guidance literature:: With hydrogenchloride; dmap; In tetrahydrofuran; methanol; acetonitrile;

Reference yield:

: 123486-10-2
2-Methoxy-4-methyl-6-(3-nitro-phenyl)-6H-pyrimidine-1,5-dicarboxylic acid 1-tert-butyl ester 5-ethyl ester

: 108930-65-0
3,6-dihydro-4-methyl-6-(3-nitrophenyl)-2-oxo-1,5-pyrimidinedicarboxylic acid 1-(1,1-dimethylethyl) 5-ethyl diester

Guidance literature:: With hydrogenchloride; In methanol; for 0.5h; Ambient temperature;
DOI:10.1021/jo00286a020

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: 108930-65-0
3,6-dihydro-4-methyl-6-(3-nitrophenyl)-2-oxo-1,5-pyrimidinedicarboxylic acid 1-(1,1-dimethylethyl) 5-ethyl diester

Guidance literature:: Multi-step reaction with 2 steps

1: 4-(dimethylamino)pyridine / acetonitrile / 1 h / Ambient temperature

2: 792 mg / 2 N aq. HCl / methanol / 0.5 h / Ambient temperature

With hydrogenchloride; dmap; In methanol; acetonitrile;
DOI:10.1021/jo00286a020