[Zn(2-[N'-(1-acetyl-2-oxopropylidene)hydrazino]benzoic acid(-1H))2(2,2'-bipyridine)]

Base Information

Chemical Name:[Zn(2-[N'-(1-acetyl-2-oxopropylidene)hydrazino]benzoic acid(-1H))2(2,2'-bipyridine)]
CAS No.:1421765-20-9
Molecular Formula:C₃₄H₃₀N₆O₈Zn
Molecular Weight:716.038
Hs Code.:

Synonyms:[Zn(2-[N'-(1-acetyl-2-oxopropylidene)hydrazino]benzoic acid(-1H))2(2,2'-bipyridine)]

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Chemical Property of [Zn(2-[N'-(1-acetyl-2-oxopropylidene)hydrazino]benzoic acid(-1H))2(2,2'-bipyridine)]

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Technology Process of [Zn(2-[N'-(1-acetyl-2-oxopropylidene)hydrazino]benzoic acid(-1H))2(2,2'-bipyridine)]

There total 2 articles about [Zn(2-[N'-(1-acetyl-2-oxopropylidene)hydrazino]benzoic acid(-1H))2(2,2'-bipyridine)] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 57.0%

: 74568-19-7
2-(2-(2,4-dioxopentan-3-ylidene)hydrazineyl) benzoic acid

: Zn(2,2'-bipyridine)(NO3)2·2H2O

: 1421765-20-9
[Zn(2-[N'-(1-acetyl-2-oxopropylidene)hydrazino]benzoic acid(-1H))2(2,2'-bipyridine)]

Guidance literature:: In ethanol; N,N-dimethyl-formamide; at 50 ℃; for 18.5h; Reflux;
DOI:10.1016/j.poly.2012.11.012

Reference yield:

: 118-92-3,159201-01-1,50816-84-7,80206-34-4,104809-47-4
anthranilic acid

: 123-54-6,81235-32-7
acetylacetone

: 1421765-20-9
[Zn(2-[N'-(1-acetyl-2-oxopropylidene)hydrazino]benzoic acid(-1H))2(2,2'-bipyridine)]

Guidance literature:: Multi-step reaction with 2 steps

1.1: hydrogenchloride; sodium nitrite / water / 0 - 5 °C

1.2: 1 h / 0 - 20 °C

2.1: ethanol; N,N-dimethyl-formamide / 18.5 h / 50 °C / Reflux

With hydrogenchloride; sodium nitrite; In ethanol; water; N,N-dimethyl-formamide;
DOI:10.1016/j.poly.2012.11.012