4-acetylamino-3-(2'-oxo-2'-<4-chlorophenyl>-ethyl)-aminobenzoic acid t-butyl ester

Base Information

Chemical Name:4-acetylamino-3-(2'-oxo-2'-<4-chlorophenyl>-ethyl)-aminobenzoic acid t-butyl ester
CAS No.:233671-37-9
Molecular Formula:C₂₁H₂₃ClN₂O₄
Molecular Weight:402.878
Hs Code.:

Synonyms:4-acetylamino-3-(2'-oxo-2'-<4-chlorophenyl>-ethyl)-aminobenzoic acid t-butyl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-acetylamino-3-(2'-oxo-2'-<4-chlorophenyl>-ethyl)-aminobenzoic acid t-butyl ester

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Technology Process of 4-acetylamino-3-(2'-oxo-2'-<4-chlorophenyl>-ethyl)-aminobenzoic acid t-butyl ester

There total 2 articles about 4-acetylamino-3-(2'-oxo-2'-<4-chlorophenyl>-ethyl)-aminobenzoic acid t-butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 536-38-9
4-chlorobenzoylmethyl bromide

: 197089-39-7
4-acetylamino-3-amino-benzoic acid t-butyl ester

: 233671-37-9
4-acetylamino-3-(2'-oxo-2'-<4-chlorophenyl>-ethyl)-aminobenzoic acid t-butyl ester

Guidance literature:: With sodium hydrogencarbonate; In N,N-dimethyl-formamide; Ambient temperature;
DOI:10.1016/S0223-5234(99)80055-5

Reference yield:

: 233671-44-8
4-acetylamino-3-(2'-oxo-2'-<2''-N-methylpyrrolyl>-ethyl)-aminobenzoic acid t-butyl ester

: 233671-37-9
4-acetylamino-3-(2'-oxo-2'-<4-chlorophenyl>-ethyl)-aminobenzoic acid t-butyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: cyanamide / ethanol / 30 h / Heating

2: 80 percent / NaHCO₃ / dimethylformamide / Ambient temperature

With CYANAMID; sodium hydrogencarbonate; In ethanol; N,N-dimethyl-formamide;
DOI:10.1016/S0223-5234(99)80055-5