diethyl 1-benzyl-2-oxopropyl phosphonate

Base Information

Chemical Name:diethyl 1-benzyl-2-oxopropyl phosphonate
CAS No.:53372-36-4
Molecular Formula:C₁₄H₂₁O₄P
Molecular Weight:284.292
Hs Code.:

Synonyms:diethyl 1-benzyl-2-oxopropyl phosphonate

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Chemical Property of diethyl 1-benzyl-2-oxopropyl phosphonate

Chemical Property:

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Technology Process of diethyl 1-benzyl-2-oxopropyl phosphonate

There total 7 articles about diethyl 1-benzyl-2-oxopropyl phosphonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: (1-benzyl-2-methyl-allyl)-phosphonic acid diethyl ester

: 53372-36-4
diethyl 1-benzyl-2-oxopropyl phosphonate

Guidance literature:: With dimethylsulfide; ozone; In dichloromethane;
DOI:10.1080/00397919808004906

Reference yield: 46.0%

: 1067-71-6
Diethyl (2-oxopropyl)phosphonate

: 100-39-0
benzyl bromide

: 53372-36-4
diethyl 1-benzyl-2-oxopropyl phosphonate

Guidance literature:: Diethyl (2-oxopropyl)phosphonate; With sodium hydride; In tetrahydrofuran; at 0 ℃; for 0.5h; Inert atmosphere;

benzyl bromide; In tetrahydrofuran; at 0 - 20 ℃; Inert atmosphere;
DOI:10.1021/acs.orglett.1c01091

Reference yield:

: 1817-57-8
4-phenyl-3-butyne-2-one

: 122-52-1
triethyl phosphite

: 53372-36-4
diethyl 1-benzyl-2-oxopropyl phosphonate

: C₁₈H₃₀O₇P₂

Guidance literature:: With nickel(II) chloride hexahydrate; In neat (no solvent); at 160 ℃; for 24h; Schlenk technique; Inert atmosphere;
DOI:10.1002/cctc.201700974