ethyl (8-((2-(diethylamino)ethyl)amino)-2,3-diphenylpyrido[2,3-b]pyrazin-6-yl)carbamate

Base Information

Chemical Name:ethyl (8-((2-(diethylamino)ethyl)amino)-2,3-diphenylpyrido[2,3-b]pyrazin-6-yl)carbamate
CAS No.:1347749-94-3
Molecular Formula:C₂₈H₃₂N₆O₂
Molecular Weight:484.601
Hs Code.:

Synonyms:ethyl (8-((2-(diethylamino)ethyl)amino)-2,3-diphenylpyrido[2,3-b]pyrazin-6-yl)carbamate

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Chemical Property of ethyl (8-((2-(diethylamino)ethyl)amino)-2,3-diphenylpyrido[2,3-b]pyrazin-6-yl)carbamate

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Technology Process of ethyl (8-((2-(diethylamino)ethyl)amino)-2,3-diphenylpyrido[2,3-b]pyrazin-6-yl)carbamate

There total 4 articles about ethyl (8-((2-(diethylamino)ethyl)amino)-2,3-diphenylpyrido[2,3-b]pyrazin-6-yl)carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 49.0%

: 1347749-90-9
C₁₄H₂₆N₆O₂

: 134-81-6
benzil

: 1347749-94-3
ethyl (8-((2-(diethylamino)ethyl)amino)-2,3-diphenylpyrido[2,3-b]pyrazin-6-yl)carbamate

Guidance literature:: In ethanol; at 20 ℃; for 40h; Inert atmosphere; Reflux;
DOI:10.1016/j.bmc.2011.09.062

Reference yield:

: 1347749-87-4
ethyl 6-amino-4-[[2-(diethylamino)-ethyl]-amino]-5-nitro-2-pyridinecarbamate

: 1347749-94-3
ethyl (8-((2-(diethylamino)ethyl)amino)-2,3-diphenylpyrido[2,3-b]pyrazin-6-yl)carbamate

Guidance literature:: Multi-step reaction with 2 steps

1: hydrogen / ethanol / 20 °C / 760.05 Torr

2: ethanol / 40 h / 20 °C / Inert atmosphere; Reflux

With hydrogen; In ethanol;
DOI:10.1016/j.bmc.2011.09.062

Reference yield:

: 6506-86-1
ethyl (6-amino-4-chloro-5-nitropyridin-2-yl)carbamate

: 1347749-94-3
ethyl (8-((2-(diethylamino)ethyl)amino)-2,3-diphenylpyrido[2,3-b]pyrazin-6-yl)carbamate

Guidance literature:: Multi-step reaction with 3 steps

1.1: ethanol / Inert atmosphere; Reflux

1.2: Column chromatography

2.1: hydrogen / ethanol / 20 °C / 760.05 Torr

3.1: ethanol / 40 h / 20 °C / Inert atmosphere; Reflux

With hydrogen; In ethanol;
DOI:10.1016/j.bmc.2011.09.062