C₅₆H₉₁N₇O₁₆Si

Base Information

Chemical Name:C₅₆H₉₁N₇O₁₆Si
CAS No.:343333-02-8
Molecular Formula:C₅₆H₉₁N₇O₁₆Si
Molecular Weight:1146.46
Hs Code.:

C<sub>56</sub>H<sub>91</sub>N<sub>7</sub>O<sub>16</sub>Si

Synonyms:C₅₆H₉₁N₇O₁₆Si

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Chemical Property of C₅₆H₉₁N₇O₁₆Si

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Technology Process of C₅₆H₉₁N₇O₁₆Si

There total 3 articles about C₅₆H₉₁N₇O₁₆Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 343332-96-7
C₄₂H₆₉N₅O₁₄

: 89106-03-6
6-benzyloxycarbonylamino-2-L-amino-hexanoic acid trimethylsilyl ethyl ester

: 104-15-4
toluene-4-sulfonic acid

: 343333-02-8
C₅₆H₉₁N₇O₁₆Si

Guidance literature:: C₄₂H₆₉N₅O₁₄; toluene-4-sulfonic acid; In methanol; at 20 ℃; for 5h;

With Dess-Martin periodane; In dichloromethane; at 20 ℃; for 2h;

6-benzyloxycarbonylamino-2-L-amino-hexanoic acid trimethylsilyl ethyl ester; With sodium tris(acetoxy)borohydride; N-ethyl-N,N-diisopropylamine; In 1,2-dichloro-ethane; at 20 ℃; for 12h; Further stages.;
DOI:10.1021/ja005886l

Reference yield:

: 2916-68-9
2-(Trimethylsilyl)ethanol

: 343333-02-8
C₅₆H₉₁N₇O₁₆Si

Guidance literature:: Multi-step reaction with 2 steps

1.1: DCC; DMAP / CH₂Cl₂ / 22 h / 20 °C

1.2: 95 percent / TFA / CH₂Cl₂ / 1.5 h / 20 °C

2.1: methanol / 5 h / 20 °C

2.2: Dess-Martin reagent / CH₂Cl₂ / 2 h / 20 °C

2.3: sodium triacetoxy-borohydride; diisopropylethylamine / 1,2-dichloro-ethane / 12 h / 20 °C

With dmap; dicyclohexyl-carbodiimide; In methanol; dichloromethane;
DOI:10.1021/ja005886l

Reference yield:

: 2389-45-9
Boc-Lys(Z)-OH

: 343333-02-8
C₅₆H₉₁N₇O₁₆Si

Guidance literature:: Multi-step reaction with 2 steps

1.1: DCC; DMAP / CH₂Cl₂ / 22 h / 20 °C

1.2: 95 percent / TFA / CH₂Cl₂ / 1.5 h / 20 °C

2.1: methanol / 5 h / 20 °C

2.2: Dess-Martin reagent / CH₂Cl₂ / 2 h / 20 °C

2.3: sodium triacetoxy-borohydride; diisopropylethylamine / 1,2-dichloro-ethane / 12 h / 20 °C

With dmap; dicyclohexyl-carbodiimide; In methanol; dichloromethane;
DOI:10.1021/ja005886l