butylcycloheptanone

Base Information

• Chemical Name: butylcycloheptanone
• CAS No.: 13152-41-5
• Molecular Formula: C₁₁H₂₂
• Molecular Weight: 154.296
• Mol file: 13152-41-5.mol

Synonyms:butylcycloheptanone

Chemical Property of butylcycloheptanone

Chemical Property:

Purity/Quality:

Safty Information:

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Technology Process of butylcycloheptanone

There total 4 articles about butylcycloheptanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

2-butyloct-7-enenitrile (1036741-73-7) → butylcycloheptanone (13152-41-5) + 1-butyl-2-methylcyclohexane (72993-33-0)

Guidance literature:

With potassium; tert-butyl alcohol; In N,N,N,N,N,N-hexamethylphosphoric triamide; diethyl ether; at 0 ℃; for 3h;

DOI:10.1021/jo800640j

Reference yield:

iodocycloheptane (2404-36-6) + butyl magnesium bromide (693-04-9) → octane (111-65-9) + Cycloheptene (628-92-2,45509-99-7) + butylcycloheptanone (13152-41-5)

Guidance literature:

With C₃₂H₃₀ClN₂NiP; In tetrahydrofuran; N,N-dimethyl acetamide; at -20 ℃; for 2h; Inert atmosphere;

DOI:10.1021/ja200270k

Reference yield:

iodocycloheptane (2404-36-6) + butyl magnesium bromide (693-04-9) → Cycloheptene (628-92-2,45509-99-7) + butylcycloheptanone (13152-41-5) + bicycloheptane (23183-11-1)

Guidance literature:

With NiCl(2,4-lutidine)(Me₂NC₆H₄NC₆H₄Ph); In tetrahydrofuran; N,N-dimethyl acetamide; at -20 ℃; for 2h; Inert atmosphere;

DOI:10.1021/ja200270k

upstream raw materials:

2-butyloct-7-enenitrile

iodocycloheptane

butyl magnesium bromide

Downstream raw materials:

1-methyl-1-butylcyclohexane

1-butylbenzene

2-butyltoluene