4-{[6-(4-tert-butyl-cyclohexyloxy)-8-methyl-naphthalen-2-ylmethyl]-amino}-butyric acid

Base Information

Chemical Name:4-{[6-(4-tert-butyl-cyclohexyloxy)-8-methyl-naphthalen-2-ylmethyl]-amino}-butyric acid
CAS No.:1266120-15-3
Molecular Formula:C₂₆H₃₇NO₃
Molecular Weight:411.585
Hs Code.:

Synonyms:4-{[6-(4-tert-butyl-cyclohexyloxy)-8-methyl-naphthalen-2-ylmethyl]-amino}-butyric acid

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Chemical Property of 4-{[6-(4-tert-butyl-cyclohexyloxy)-8-methyl-naphthalen-2-ylmethyl]-amino}-butyric acid

Chemical Property:

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Technology Process of 4-{[6-(4-tert-butyl-cyclohexyloxy)-8-methyl-naphthalen-2-ylmethyl]-amino}-butyric acid

There total 9 articles about 4-{[6-(4-tert-butyl-cyclohexyloxy)-8-methyl-naphthalen-2-ylmethyl]-amino}-butyric acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₆H₃₅NO₃

: 1266120-15-3
4-{[6-(4-tert-butyl-cyclohexyloxy)-8-methyl-naphthalen-2-ylmethyl]-amino}-butyric acid

Guidance literature:: With ethanol; sodium cyanoborohydride; at 20 - 50 ℃;

Reference yield:

: 57404-87-2
3-methoxy-1-methylnaphthalene

: 1266120-15-3
4-{[6-(4-tert-butyl-cyclohexyloxy)-8-methyl-naphthalen-2-ylmethyl]-amino}-butyric acid

Guidance literature:: Multi-step reaction with 5 steps

1.1: tetra-(n-butyl)ammonium iodide; boron trichloride / dichloromethane / 1.08 h / -78 - 0 °C / Inert atmosphere

2.1: caesium carbonate / butanone; tert-butyl alcohol / 80 °C

3.1: tin(IV) chloride / 1,2-dichloro-ethane / 1 h / 0 °C

3.2: 1 h / 0 - 20 °C

3.3: Cooling with ice

4.1: ethanol / 2 h / Reflux

5.1: ethanol; sodium cyanoborohydride / 20 - 50 °C

With ethanol; boron trichloride; tin(IV) chloride; tetra-(n-butyl)ammonium iodide; sodium cyanoborohydride; caesium carbonate; In ethanol; dichloromethane; 1,2-dichloro-ethane; butanone; tert-butyl alcohol;

Reference yield:

: 123-54-6,81235-32-7
acetylacetone

: 1266120-15-3
4-{[6-(4-tert-butyl-cyclohexyloxy)-8-methyl-naphthalen-2-ylmethyl]-amino}-butyric acid

Guidance literature:: Multi-step reaction with 7 steps

1.1: toluene-4-sulfonic acid / methanol / 5 h / 55 °C

2.1: sodium t-butanolate / tetrahydrofuran / 2 h / 30 - 45 °C

2.2: 6 h / 55 °C

3.1: tetra-(n-butyl)ammonium iodide; boron trichloride / dichloromethane / 1.08 h / -78 - 0 °C / Inert atmosphere

4.1: caesium carbonate / butanone; tert-butyl alcohol / 80 °C

5.1: tin(IV) chloride / 1,2-dichloro-ethane / 1 h / 0 °C

5.2: 1 h / 0 - 20 °C

5.3: Cooling with ice

6.1: ethanol / 2 h / Reflux

7.1: ethanol; sodium cyanoborohydride / 20 - 50 °C

With ethanol; boron trichloride; tin(IV) chloride; tetra-(n-butyl)ammonium iodide; sodium cyanoborohydride; caesium carbonate; toluene-4-sulfonic acid; sodium t-butanolate; In tetrahydrofuran; methanol; ethanol; dichloromethane; 1,2-dichloro-ethane; butanone; tert-butyl alcohol;