tert-butyldimethylsilyl 2-azido-3-O-benzyl-4,6-O-benzylidene-β-D-galactopyranoside

Base Information

Chemical Name:tert-butyldimethylsilyl 2-azido-3-O-benzyl-4,6-O-benzylidene-β-D-galactopyranoside
CAS No.:158421-28-4
Molecular Formula:C₂₆H₃₅N₃O₅Si
Molecular Weight:497.667
Hs Code.:

Synonyms:tert-butyldimethylsilyl 2-azido-3-O-benzyl-4,6-O-benzylidene-β-D-galactopyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of tert-butyldimethylsilyl 2-azido-3-O-benzyl-4,6-O-benzylidene-β-D-galactopyranoside

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Technology Process of tert-butyldimethylsilyl 2-azido-3-O-benzyl-4,6-O-benzylidene-β-D-galactopyranoside

There total 1 articles about tert-butyldimethylsilyl 2-azido-3-O-benzyl-4,6-O-benzylidene-β-D-galactopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 100-39-0
benzyl bromide

: 147254-13-5
(tert-butyldimethyl)silyl 2-azido-4,6-O-benzylidene-2-deoxy-β-D-galactopyranoside

: 158421-28-4
tert-butyldimethylsilyl 2-azido-3-O-benzyl-4,6-O-benzylidene-β-D-galactopyranoside

Guidance literature:: With sodium hydride; Yield given. Multistep reaction; 1.) THF, 23 deg C, 15 min, 2.) THF, 60 deg C, 10 h;
DOI:10.1021/ja00090a018

Reference yield: 98.0%

: 158421-28-4
tert-butyldimethylsilyl 2-azido-3-O-benzyl-4,6-O-benzylidene-β-D-galactopyranoside

: 158421-32-0
tert-butyldimethylsilyl 2-amino-3-O-benzyl-4,6-O-benzylidene-β-D-galactopyranoside

Guidance literature:: With pyridine; hydrogen sulfide; triethylamine; at 23 ℃; for 20h;
DOI:10.1021/ja00090a018

Reference yield:

: 158421-28-4
tert-butyldimethylsilyl 2-azido-3-O-benzyl-4,6-O-benzylidene-β-D-galactopyranoside

: (2S,4aR,6R,7R,8R,8aR)-7-Azido-8-benzyloxy-2-phenyl-hexahydro-pyrano[3,2-d][1,3]dioxin-6-ol

: (2S,4aR,6S,7R,8R,8aR)-7-Azido-8-benzyloxy-2-phenyl-hexahydro-pyrano[3,2-d][1,3]dioxin-6-ol

Guidance literature:: With potassium fluoride; In methanol; at 23 ℃; for 7h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
DOI:10.1021/ja00090a018