[2-(tert-Butyl-diphenyl-silanyloxy)-ethyl]-(1-methyl-1-phenyl-ethyl)-amine

Base Information

• Chemical Name: [2-(tert-Butyl-diphenyl-silanyloxy)-ethyl]-(1-methyl-1-phenyl-ethyl)-amine
• CAS No.: 179096-88-9
• Molecular Formula: C₂₇H₃₅NOSi
• Molecular Weight: 417.666

Synonyms:[2-(tert-Butyl-diphenyl-silanyloxy)-ethyl]-(1-methyl-1-phenyl-ethyl)-amine

Chemical Property of [2-(tert-Butyl-diphenyl-silanyloxy)-ethyl]-(1-methyl-1-phenyl-ethyl)-amine

Chemical Property:

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Technology Process of [2-(tert-Butyl-diphenyl-silanyloxy)-ethyl]-(1-methyl-1-phenyl-ethyl)-amine

There total 2 articles about [2-(tert-Butyl-diphenyl-silanyloxy)-ethyl]-(1-methyl-1-phenyl-ethyl)-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 54.0%

tert-butylchlorodiphenylsilane (58479-61-1) + 2-(1-Methyl-1-phenyl-ethylamino)-ethanol (158434-50-5) → [2-(tert-Butyl-diphenyl-silanyloxy)-ethyl]-(1-methyl-1-phenyl-ethyl)-amine (179096-88-9)

Guidance literature:

With triethylamine; In dichloromethane; for 2.5h; Ambient temperature;

DOI:10.1021/jm960092w

Reference yield:

2-phenyl-2-propylamine (585-32-0) → [2-(tert-Butyl-diphenyl-silanyloxy)-ethyl]-(1-methyl-1-phenyl-ethyl)-amine (179096-88-9)

Guidance literature:

Multi-step reaction with 2 steps

1: 1.) LiClO₄ / 1.) THF, 0 deg C, 10 min, 2.) THF, CH₃CN, RT, 3 h

2: 54 percent / Et₃N / CH₂Cl₂ / 2.5 h / Ambient temperature

With lithium perchlorate; triethylamine; In dichloromethane;

DOI:10.1021/jm960092w

Reference yield: 67.0%

2,5-dimethylbenzoyl chloride (22328-43-4) + [2-(tert-Butyl-diphenyl-silanyloxy)-ethyl]-(1-methyl-1-phenyl-ethyl)-amine (179096-88-9) → N-[2-(tert-Butyl-diphenyl-silanyloxy)-ethyl]-2,5-dimethyl-N-(1-methyl-1-phenyl-ethyl)-benzamide (179096-91-4)

Guidance literature:

With triethylamine; In dichloromethane; for 19h; Ambient temperature;

DOI:10.1021/jm960092w

upstream raw materials:

tert-butylchlorodiphenylsilane

2-(1-Methyl-1-phenyl-ethylamino)-ethanol

2-phenyl-2-propylamine

Downstream raw materials:

N-[2-(tert-Butyl-diphenyl-silanyloxy)-ethyl]-2,5-dimethyl-N-(1-methyl-1-phenyl-ethyl)-benzamide

N-[2-(tert-Butyl-diphenyl-silanyloxy)-ethyl]-5-chloro-2-methyl-N-(1-methyl-1-phenyl-ethyl)-benzamide

N-[2-(tert-Butyl-diphenyl-silanyloxy)-ethyl]-2-methyl-N-(1-methyl-1-phenyl-ethyl)-benzamide

N-[2-(tert-Butyl-diphenyl-silanyloxy)-ethyl]-2-(3-hydroxy-propyl)-N-(1-methyl-1-phenyl-ethyl)-benzamide

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