2,5-Dimethylbenzoyl chloride

Base Information

Chemical Name:2,5-Dimethylbenzoyl chloride
CAS No.:22328-43-4
Molecular Formula:C9H9 Cl O
Molecular Weight:168.623
Hs Code.:2916399090
European Community (EC) Number:824-139-9
DSSTox Substance ID:DTXSID50493387
Wikidata:Q82340036
Mol file:22328-43-4.mol

Synonyms:2,5-Dimethylbenzoyl chloride;22328-43-4;2,5-dimethylbenzoylchloride;Benzoyl chloride, 2,5-dimethyl- (6CI,7CI,8CI,9CI);2, 5-dimethylbenzoyl chloride;SCHEMBL1311663;DTXSID50493387;MGBRPGMQNVRQCG-UHFFFAOYSA-N;XAA32843;MFCD00045218;AKOS007930321;FS-5022;2,5-dimethyl-1-benzenecarbonyl chloride;EN300-78737;F81616;A816113

Suppliers and Price of 2,5-Dimethylbenzoyl chloride

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
2,5-DimethylbenzoylChloride
100mg
$ 60.00

TRC
2,5-DimethylbenzoylChloride
50mg
$ 45.00

Rieke Metals
2,5-DIMETHYLBENZOYLCHLORIDE
5g
$ 1943.00

Rieke Metals
2,5-DIMETHYLBENZOYLCHLORIDE
1g
$ 809.00

Matrix Scientific
2,5-Dimethylbenzoylchloride 97%
10g
$ 1106.00

Matrix Scientific
2,5-Dimethylbenzoylchloride 97%
1g
$ 179.00

Labseeker
BENZOYLCHLORIDE,2,5-DIMETHYL- 95
50g
$ 2475.00

Atlantic Research Chemicals
2,5-Dimethylbenzoylchloride 95%
10gm:
$ 459.49

American Custom Chemicals Corporation
2,5-DIMETHYLBENZOYL CHLORIDE 95.00%
2.5G
$ 1227.82

American Custom Chemicals Corporation
2,5-DIMETHYLBENZOYL CHLORIDE 95.00%
1G
$ 852.55

Total 6 raw suppliers

Chemical Property of 2,5-Dimethylbenzoyl chloride

Chemical Property:

Boiling Point:239.3±9.0 °C(Predicted)
PSA：17.07000
Density:1.136±0.06 g/cm3(Predicted)
LogP:2.68240
XLogP3:3.2
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:1
Exact Mass:168.0341926
Heavy Atom Count:11
Complexity:156

Purity/Quality:

99%, ^*data from raw suppliers

2,5-DimethylbenzoylChloride ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=CC(=C(C=C1)C)C(=O)Cl

Technology Process of 2,5-Dimethylbenzoyl chloride

There total 7 articles about 2,5-Dimethylbenzoyl chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 610-72-0
2,5-dimethylbenzoic acid

: 22328-43-4
2,5-dimethylbenzoyl chloride

Guidance literature:: With oxalyl dichloride; In dichloromethane; N,N-dimethyl-formamide; at 20 ℃; for 1h;
DOI:10.1055/s-2004-834861

Reference yield:

: 79-37-8
oxalyl dichloride

: 106-42-3
para-xylene

: 22328-43-4
2,5-dimethylbenzoyl chloride

Guidance literature:: With aluminium trichloride; In dichloromethane; at 10 ℃; for 0.5h;
DOI:10.1021/jo991055q

Reference yield:

: 106-42-3
para-xylene

: 22328-43-4
2,5-dimethylbenzoyl chloride

Guidance literature:: Multi-step reaction with 3 steps

1: AlCl₃; carbon disulfide

2: aqueous potassium hypochlorite solution / 60 - 70 °C

3: thionyl chloride

With carbon disulfide; aluminium trichloride; thionyl chloride; potassium hypochlorite;
DOI:10.1021/ja01303a006