[CH₃C₁₁H₇NPC₆H₅]⁽¹⁺⁾*O₃SCF₃^(1-)=[CH₃C₁₁H₇NPC₆H₅]O₃SCF₃

Base Information

• Chemical Name: [CH₃C₁₁H₇NPC₆H₅]⁽¹⁺⁾*O₃SCF₃^(1-)=[CH₃C₁₁H₇NPC₆H₅]O₃SCF₃
• CAS No.: 1312012-43-3
• Molecular Formula: CF₃O₃S*C₁₈H₁₅NP
• Molecular Weight: 425.368

Synonyms:[CH₃C₁₁H₇NPC₆H₅]⁽¹⁺⁾*O₃SCF₃^(1-)=[CH₃C₁₁H₇NPC₆H₅]O₃SCF₃

Chemical Property of [CH₃C₁₁H₇NPC₆H₅]⁽¹⁺⁾*O₃SCF₃^(1-)=[CH₃C₁₁H₇NPC₆H₅]O₃SCF₃

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Technology Process of [CH₃C₁₁H₇NPC₆H₅]⁽¹⁺⁾*O₃SCF₃^(1-)=[CH₃C₁₁H₇NPC₆H₅]O₃SCF₃

There total 5 articles about [CH₃C₁₁H₇NPC₆H₅]⁽¹⁺⁾*O₃SCF₃^(1-)=[CH₃C₁₁H₇NPC₆H₅]O₃SCF₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

C17H12NP (1312012-30-8) + methyl trifluoromethanesulfonate (333-27-7) → [CH3C11H7NPC6H5](1+)*O3SCF3(1-)=[CH3C11H7NPC6H5]O3SCF3 (1312012-43-3)

Guidance literature:

In dichloromethane; at 0 ℃; Inert atmosphere;

DOI:10.1021/ic200951x

Reference yield:

(2-bromophenyl)boronic acid (244205-40-1) → [CH3C11H7NPC6H5](1+)*O3SCF3(1-)=[CH3C11H7NPC6H5]O3SCF3 (1312012-43-3)

Guidance literature:

Multi-step reaction with 4 steps

1.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene / tetrahydrofuran; water / 72 h / Inert atmosphere; Reflux

2.1: phosphorus tribromide / 40 h / 140 °C / Inert atmosphere

3.1: tert.-butyl lithium / diethyl ether; pentane / 1 h / -78 °C / Inert atmosphere

3.2: -78 - 20 °C / Inert atmosphere

4.1: dichloromethane / 0 °C / Inert atmosphere

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; tert.-butyl lithium; phosphorus tribromide; potassium carbonate; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; In tetrahydrofuran; diethyl ether; dichloromethane; water; pentane; 1.1: Suzuki-Miyaura coupling;

DOI:10.1021/ic200951x

Reference yield:

2-chloro-3-iodopyridine (78607-36-0) → [CH3C11H7NPC6H5](1+)*O3SCF3(1-)=[CH3C11H7NPC6H5]O3SCF3 (1312012-43-3)

Guidance literature:

Multi-step reaction with 4 steps

1.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene / tetrahydrofuran; water / 72 h / Inert atmosphere; Reflux

2.1: phosphorus tribromide / 40 h / 140 °C / Inert atmosphere

3.1: tert.-butyl lithium / diethyl ether; pentane / 1 h / -78 °C / Inert atmosphere

3.2: -78 - 20 °C / Inert atmosphere

4.1: dichloromethane / 0 °C / Inert atmosphere

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; tert.-butyl lithium; phosphorus tribromide; potassium carbonate; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; In tetrahydrofuran; diethyl ether; dichloromethane; water; pentane; 1.1: Suzuki-Miyaura coupling;

DOI:10.1021/ic200951x

upstream raw materials:

3-(2-bromophenyl)-2-chloropyridine

2-bromo-3-(2-bromophenyl)pyridine

C₁₇H₁₂NP

methyl trifluoromethanesulfonate

Downstream raw materials:

[(CH₃C₁₁H₇NPC₆H₅)AuCl]⁽¹⁺⁾*O₃SCF₃^(1-)=[(CH₃C₁₁H₇NPC₆H₅)AuCl]O₃SCF₃

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