C₆₆H₄₇N₃

Base Information

• Chemical Name: C₆₆H₄₇N₃
• CAS No.: 1290615-04-1
• Molecular Formula: C₆₆H₄₇N₃
• Molecular Weight: 882.119
• Mol file: 1290615-04-1.mol

Synonyms:C₆₆H₄₇N₃

Chemical Property of C₆₆H₄₇N₃

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₆₆H₄₇N₃

There total 4 articles about C₆₆H₄₇N₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

2-chloro-9-(4-chlorophenyl)carbazole (1290615-01-8) + N-[1,1'-biphenyl]-2-yl-[1,1'-biphenyl]-2-amine → C66H47N3 (1290615-04-1)

Guidance literature:

With sodium t-butanolate; tri-tert-butyl phosphine; palladium diacetate; In o-xylene; at 130 ℃; for 18h; Inert atmosphere;

Reference yield:

2-nitrophenyl bromide (577-19-5) → C66H47N3 (1290615-04-1)

Guidance literature:

Multi-step reaction with 4 steps

1: potassium carbonate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / water; tetrahydrofuran / 8 h / Inert atmosphere; Reflux

2: triethyl phosphite / nitrogen / 24 h / 150 °C / Inert atmosphere

3: potassium carbonate / palladium diacetate; tri-tert-butyl phosphine / o-xylene / 24 h / 130 °C / Inert atmosphere

4: sodium t-butanolate / palladium diacetate; tri-tert-butyl phosphine / o-xylene / 18 h / 130 °C / Inert atmosphere

With potassium carbonate; sodium t-butanolate; triethyl phosphite; tetrakis(triphenylphosphine) palladium⁽⁰⁾; tri-tert-butyl phosphine; palladium diacetate; In tetrahydrofuran; o-xylene; nitrogen; water;

Reference yield:

2-chloro-9H-carbazole (10537-08-3) → C66H47N3 (1290615-04-1)

Guidance literature:

Multi-step reaction with 2 steps

1: potassium carbonate / palladium diacetate; tri-tert-butyl phosphine / o-xylene / 24 h / 130 °C / Inert atmosphere

2: sodium t-butanolate / palladium diacetate; tri-tert-butyl phosphine / o-xylene / 18 h / 130 °C / Inert atmosphere

With potassium carbonate; sodium t-butanolate; tri-tert-butyl phosphine; palladium diacetate; In o-xylene;

upstream raw materials:

2-nitrophenyl bromide

2-chloro-9H-carbazole

4'-chloro-2-nitrobiphenyl

2-chloro-9-(4-chlorophenyl)carbazole

Refernces